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2 "Hye Sung Kim"
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[Korean]
Briquetting of Waste Silicon Carbide Obtained from Silicon Wafer Sludges
Seong Mo Koo, Su Jong Yoon, Hye Sung Kim
J Korean Powder Metall Inst. 2016;23(1):43-48.   Published online February 1, 2016
DOI: https://doi.org/10.4150/KPMI.2016.23.1.43
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Waste SiC powders obtained from silicon wafer sludge have very low density and a narrow particle size distribution of 10-20 μm. A scarce yield of C and Si is expected when SiC powders are incorporated into the Fe melt without briquetting. Here, the briquetting variables of the SiC powders are studied as a function of the sintering temperature, pressure, and type and contents of the binders to improve the yield. It is experimentally confirmed that Si and C from the sintered briquette can be incorporated effectively into the Fe melt when the waste SiC powders milled for 30 min with 20 wt.% Fe binder are sintered at 1100°C upon compaction using a pressure of 250 MPa. XRF-WDS analysis shows that an yield of about 90% is obtained when the SiC briquette is kept in the Fe melt at 1650°C for more than 1 h.

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[Korean]
Effect of Sintering Temperature on the Microstructure and Mechanical Properties of Solid Oxide Fuel Cell Anode Fabricated by Spark Plasma Sintering
Byung Ju Song, Ka Ram Kim, Hye Sung Kim
J Korean Powder Metall Inst. 2013;20(6):425-431.
DOI: https://doi.org/10.4150/KPMI.2013.20.6.425
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Microstructural and mechanical properties of Ni-YSZ fabricated using SPS processing have been investigated at various sintering temperatures. Our study shows samples to be applied as a SOFC anode have the proper porosity of 40% and high hardness when processed at 1100°C. These results are comparable to the values obtained at 100-200°C higher sintering temperature reported by others. This result is important because when the fabrication processes are performed above 1100°C, the mechanical property starts to decrease drastically. This is caused by the fast grain coarsening at the higher temperature, which initiates a mismatch between thermal expansion coefficients of Ni and YSZ and induces cracks as well.

Journal of Powder Materials : Journal of Powder Materials
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