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From articles published in Journal of Powder Materials during the past two years (2023 ~ ).

Research Articles
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[Korean]
Development of Composite-film-based Flexible Energy Harvester using Lead-free BCTZ Piezoelectric Nanomaterials
Gwang Hyeon Kim, Hyeon Jun Park, Bitna Bae, Haksu Jang, Cheol Min Kim, Donghun Lee, Kwi-Il Park
J Powder Mater. 2024;31(1):16-22.   Published online February 28, 2024
DOI: https://doi.org/10.4150/KPMI.2024.31.1.16
  • 1,370 View
  • 30 Download
  • 8 Citations
AbstractAbstract PDF
Composite-based piezoelectric devices are extensively studied to develop sustainable power supply and selfpowered devices owing to their excellent mechanical durability and output performance. In this study, we design a leadfree piezoelectric nanocomposite utilizing (Ba0.85Ca0.15)(Ti0.9Zr0.1)O3 (BCTZ) nanomaterials for realizing highly flexible energy harvesters. To improve the output performance of the devices, we incorporate porous BCTZ nanowires (NWs) into the nanoparticle (NP)-based piezoelectric nanocomposite. BCTZ NPs and NWs are synthesized through the solidstate reaction and sol-gel-based electrospinning, respectively; subsequently, they are dispersed inside a polyimide matrix. The output performance of the energy harvesters is measured using an optimized measurement system during repetitive mechanical deformation by varying the composition of the NPs and NWs. A nanocomposite-based energy harvester with 4:1 weight ratio generates the maximum open-circuit voltage and short-circuit current of 0.83 V and 0.28 A, respectively. In this study, self-powered devices are constructed with enhanced output performance by using piezoelectric energy harvesting for application in flexible and wearable devices.

Citations

Citations to this article as recorded by  
  • Long‐Lasting, Steady and Enhanced Energy Harvesting by Inserting a Conductive Layer into the Piezoelectric Polymer
    HakSu Jang, Gwang Hyeon Kim, Dong Won Jeon, Hyeon Jun Park, BitNa Bae, Nagamalleswara Rao Alluri, Cheol Min Kim, Changyeon Baek, Min‐Ku Lee, Sung Beom Cho, Gyoung‐Ja Lee, Kwi‐Il Park
    Advanced Functional Materials.2025;[Epub]     CrossRef
  • Flexible hybrid thermoelectric films made of bismuth telluride-PEDOT:PSS composites enabled by freezing-thawing process and simple chemical treatment
    Cheol Min Kim, Seoha Kim, Nagamalleswara Rao Alluri, Bitna Bae, Momanyi Amos Okirigiti, Gwang Hyun Kim, Hyeon Jun Park, Haksu Jang, Changyeon Baek, Min-Ku Lee, Gyoung-Ja Lee, Kwi-Il Park
    Materials Today Chemistry.2025; 44: 102532.     CrossRef
  • Dual-controlled piezoelectric composite film with enhanced crystallinity and defect-free via solvent vapor treatment
    HakSu Jang, Hyeon Jun Park, Gwang Hyeon Kim, Cheol Min Kim, Nagamalleswara Rao Alluri, BitNa Bae, HyoMin Jeon, DongHun Lee, Kwi-Il Park
    Nano Energy.2025; 136: 110705.     CrossRef
  • Optimized Process and Mechanical and Electrical Analysis of Polyimide/Pb(Zr,Ti)O3-Based Flexible Piezoelectric Composites
    Junki Lee, Sang-il Yoon, Hyunseung Kim, Chang Kyu Jeong
    Journal of Powder Materials.2025; 32(1): 16.     CrossRef
  • Flexible Hybrid Energy Harvester based on Thermoelectric Composite Film and Electrospun Piezopolymer Membranes
    Hyomin Jeon, Cheol Min Kim, Hyeon Jun Park, Bitna Bae, Hyejeong Choi, HakSu Jang, Kwi-Il Park
    Journal of Powder Materials.2025; 32(2): 104.     CrossRef
  • Flexible Thermoelectric Energy Harvester with Stacked Structure of Thermoelectric Composite Films Made of PVDF and Bi2Te3-Based Particles
    Da Eun Shin, Nagamalleswara Rao Alluri, Kwi-Il Park
    ACS Applied Energy Materials.2024; 7(19): 8288.     CrossRef
  • Enhanced energy harvesting of fibrous composite membranes via plasma-piezopolymer interaction
    Hyeon Jun Park, Bitna Bae, HakSu Jang, Dong Yeol Hyeon, Dong Hun Lee, Gwang Hyun Kim, Cheol Min Kim, Nagamalleswara Rao Alluri, Changyeon Baek, Min-Ku Lee, Gyoung-Ja Lee, Kwi-Il Park
    Nano Energy.2024; 131: 110299.     CrossRef
  • CoFe2O4-BaTiO3 core-shell-embedded flexible polymer composite as an efficient magnetoelectric energy harvester
    Bitna Bae, Nagamalleswara Rao Alluri, Cheol Min Kim, Jungho Ryu, Gwang Hyeon Kim, Hyeon Jun Park, Changyeon Baek, Min-Ku Lee, Gyoung-Ja Lee, Geon-Tae Hwang, Kwi-Il Park
    Materials Today Physics.2024; 48: 101567.     CrossRef
Article image
[English]
Microstructural Evolution and Mechanical Properties of Ti-6Al-4V Alloy through Selective Laser Melting: Comprehensive Study on the Effect of Hot Isostatic Pressing (HIP)
Gargi Roy, Raj Narayan Hajra, Woo Hyeok Kim, Jongwon Lee, Sangwoo Kim, Jeoung Han Kim
J Powder Mater. 2024;31(1):1-7.   Published online February 28, 2024
DOI: https://doi.org/10.4150/KPMI.2024.31.1.1
  • 5,113 View
  • 122 Download
  • 8 Citations
AbstractAbstract PDF

This study explores the profound impact of varying oxygen content on microstructural and mechanical properties in specimens HO and LO. The higher oxygen concentration in specimen HO is found to significantly influence alpha lath sizes, resulting in a size of 0.5-1 μm, contrasting with the 1-1.5 μm size observed in specimen LO. Pore fraction, governed by oxygen concentration, is high in specimen HO, registering a value of 0.11%, whereas specimen LO exhibits a lower pore fraction (0.02%). Varied pore types in each specimen further underscore the role of oxygen concentration in shaping microstructural morphology. Despite these microstructural variations, the average hardness remains consistent at ~370 HV. This study emphasizes the pivotal role of oxygen content in influencing microstructural features, contributing to a comprehensive understanding of the intricate interplay between elemental composition and material properties.

Citations

Citations to this article as recorded by  
  • Mechanical response and microstructural evolution of a composite joint fabricated by green laser dissimilar welding of VCoNi medium entropy alloy and 17-4PH stainless steel
    Hadiseh Esmaeilpoor, Mahdi Aghaahmadi, Hyun Jong Yoo, Chan Woong Park, Tae Jin Jang, Seok Su Sohn, Jeoung Han Kim
    Journal of Materials Science & Technology.2025; 213: 223.     CrossRef
  • High-integrity diffusion bonding of laser powder bed fused, forged, and rolled Ti–6Al–4V alloys
    Seoyeon Jeon, Hyunjong Ha, Dong Jun Lee, Hyeonil Park, Yong Nam Kwon, Hyunjoo Choi, Hyokyung Sung
    Journal of Materials Research and Technology.2025; 35: 2108.     CrossRef
  • Removal of Organic and Inorganic Contaminants from Titanium Turning Scrap via Alkali and Acid Two-Step Cleaning
    Seong Min An, Raj Narayan Hajra, Chan Hee Park, Jin-Ho Yoon, Jinsung Rho, Chang-Min Yoon, Jeoung Han Kim
    MATERIALS TRANSACTIONS.2025; 66(7): 855.     CrossRef
  • Effect of Support Structure on Residual Stress Distribution in Ti-6Al-4V Alloy Fabricated by Laser Powder Bed Fusion
    Seungyeon Lee, Haeum Park, Min Jae Baek, Dong Jun Lee, Jae Wung Bae, Ji-Hun Yu, Jeong Min Park
    Journal of Powder Materials.2025; 32(3): 244.     CrossRef
  • Obtaining functionally-graded metal-matrix materials Ti‒6Al‒4V + WC in the process of 3D printing by the method of additive plasma-arc deposition
    V. Korzhyk, A. Grynyuk, O. Babych, O. Berdnikova, Ye. Illiashenko, O. Bushma
    The Paton Welding Journal.2025; 2025(8): 29.     CrossRef
  • Obtaining functionally-graded metal-matrix materials ti‒6al‒4v + wc by the method of additive plasma-arc deposition
    V.M. Korzhyk, A.A. Grynyuk, O.A. Babych, O.M. Berdnikova, Ye.V. Illiashenko, O.I. Bushma
    Avtomatičeskaâ svarka (Kiev).2025; 2025(5): 48.     CrossRef
  • Comparative Review of the Microstructural and Mechanical Properties of Ti-6Al-4V Fabricated via Wrought and Powder Metallurgy Processes
    Raj Narayan Hajra, Gargi Roy, An Seong Min, Hyunseok Lee, Jeoung Han Kim
    Journal of Powder Materials.2024; 31(5): 365.     CrossRef
  • A Parametric Study on the L-PBF Process of an AlSi10Mg Alloy for High-Speed Productivity of Automotive Prototype Parts
    Yeonha Chang, Hyomoon Joo, Wanghyun Yong, Yeongcheol Jo, Seongjin Kim, Hanjae Kim, Yeon Woo Kim, Kyung Tae Kim, Jeong Min Park
    Journal of Powder Materials.2024; 31(5): 390.     CrossRef
Article
Article image
[Korean]
Effect of Bulk Shape on Mechanical Properties of Ti-6Al-4V Alloy Manufactured by Laser Powder Bed Fusion
Haeum Park, Yeon Woo Kim, Seungyeon Lee, Kyung Tae Kim, Ji-Hun Yu, Jung Gi Kim, Jeong Min Park
J Powder Mater. 2023;30(2):140-145.   Published online April 1, 2023
DOI: https://doi.org/10.4150/KPMI.2023.30.2.140
  • 2,159 View
  • 29 Download
  • 6 Citations
AbstractAbstract PDF

Although the Ti–6Al–4V alloy has been used in the aircraft industry owing to its excellent mechanical properties and low density, the low formability of the alloy hinders broadening its applications. Recently, laser-powder bed fusion (L-PBF) has become a novel process for overcoming the limitations of the alloy (i.e., low formability), owing to the high degree of design freedom for the geometry of products having outstanding performance used in hightech applications. In this study, to investigate the effect of bulk shape on the microstructure and mechanical properties of L-PBFed Ti-6Al-4V alloys, two types of samples are fabricated using L-PBF: thick and thin samples. The thick sample exhibits lower strength and higher ductility than the thin sample owing to the larger grain size and lower residual dislocation density of the thick sample because of the heat input during the L-PBF process.

Citations

Citations to this article as recorded by  
  • Effect of Support Structure on Residual Stress Distribution in Ti-6Al-4V Alloy Fabricated by Laser Powder Bed Fusion
    Seungyeon Lee, Haeum Park, Min Jae Baek, Dong Jun Lee, Jae Wung Bae, Ji-Hun Yu, Jeong Min Park
    Journal of Powder Materials.2025; 32(3): 244.     CrossRef
  • Cryogenic Tensile Behavior of Ferrous Medium-entropy Alloy Additively Manufactured by Laser Powder Bed Fusion
    Seungyeon Lee, Kyung Tae Kim, Ji-Hun Yu, Hyoung Seop Kim, Jae Wung Bae, Jeong Min Park
    journal of Korean Powder Metallurgy Institute.2024; 31(1): 8.     CrossRef
  • Microstructural Evolution and Mechanical Properties of Ti-6Al-4V Alloy through Selective Laser Melting: Comprehensive Study on the Effect of Hot Isostatic Pressing (HIP)
    Gargi Roy, Raj Narayan Hajra, Woo Hyeok Kim, Jongwon Lee, Sangwoo Kim, Jeoung Han Kim
    journal of Korean Powder Metallurgy Institute.2024; 31(1): 1.     CrossRef
  • Data-driven Approach to Explore the Contribution of Process Parameters for Laser Powder Bed Fusion of a Ti-6Al-4V Alloy
    Jeong Min Park, Jaimyun Jung, Seungyeon Lee, Haeum Park, Yeon Woo Kim, Ji-Hun Yu
    journal of Korean Powder Metallurgy Institute.2024; 31(2): 137.     CrossRef
  • A Parametric Study on the L-PBF Process of an AlSi10Mg Alloy for High-Speed Productivity of Automotive Prototype Parts
    Yeonha Chang, Hyomoon Joo, Wanghyun Yong, Yeongcheol Jo, Seongjin Kim, Hanjae Kim, Yeon Woo Kim, Kyung Tae Kim, Jeong Min Park
    Journal of Powder Materials.2024; 31(5): 390.     CrossRef
  • High-speed manufacturing-driven strength-ductility improvement of H13 tool steel fabricated by selective laser melting
    Yeon Woo Kim, Haeum Park, Young Seong Eom, Dong Gill Ahn, Kyung Tae Kim, Ji-hun Yu, Yoon Suk Choi, Jeong Min Park
    Powder Metallurgy.2023; 66(5): 582.     CrossRef
Research Articles
Article image
[English]
Exploring Thermoelectric Transport Properties and Band Parameters of n-Type Bi2-xSbxTe3 Compounds Using the Single Parabolic Band Model
Linh Ba Vu, Soo-ho Jung, Jinhee Bae, Jong Min Park, Kyung Tae Kim, Injoon Son, Seungki Jo
J Powder Mater. 2024;31(2):119-125.   Published online April 30, 2024
DOI: https://doi.org/10.4150/jpm.2024.00045
  • 2,513 View
  • 77 Download
  • 5 Citations
AbstractAbstract PDF
The n-type Bi2-xSbxTe3 compounds have been of great interest due to its potential to achieve a high thermoelectric performance, comparable to that of p-type Bi2-xSbxTe3. However, a comprehensive understanding on the thermoelectric properties remains lacking. Here, we investigate the thermoelectric transport properties and band characteristics of n-type Bi2-xSbxTe3 (x = 0.1 – 1.1) based on experimental and theoretical considerations. We find that the higher power factor at lower Sb content results from the optimized balance between the density of state effective mass and nondegenerate mobility. Additionally, a higher carrier concentration at lower x suppresses bipolar conduction, thereby reducing thermal conductivity at elevated temperatures. Consequently, the highest zT of ~ 0.5 is observed at 450 K for x = 0.1 and, according to the single parabolic band model, it could be further improved by ~70 % through carrier concentration tuning.

Citations

Citations to this article as recorded by  
  • Review of “Integrated Computer-Aided Process Engineering Session in the 17th International Symposium on Novel and Nano Materials (ISNNM, 14–18 November 2022)”
    Yeon-Joo Lee, Pil-Ryung Cha, Hyoung-Seop Kim, Hyun-Joo Choi
    MATERIALS TRANSACTIONS.2025; 66(1): 144.     CrossRef
  • Enhanced energy harvesting performance of bendable thermoelectric generator enabled by trapezoidal-shaped legs
    Momanyi Amos Okirigiti, Cheol Min Kim, Hyejeong Choi, Nagamalleswara Rao Alluri, Changyeon Baek, Min-Ku Lee, Gyoung-Ja Lee, Kwi-Il Park
    Journal of Power Sources.2025; 631: 236254.     CrossRef
  • Flexible hybrid thermoelectric films made of bismuth telluride-PEDOT:PSS composites enabled by freezing-thawing process and simple chemical treatment
    Cheol Min Kim, Seoha Kim, Nagamalleswara Rao Alluri, Bitna Bae, Momanyi Amos Okirigiti, Gwang Hyun Kim, Hyeon Jun Park, Haksu Jang, Changyeon Baek, Min-Ku Lee, Gyoung-Ja Lee, Kwi-Il Park
    Materials Today Chemistry.2025; 44: 102532.     CrossRef
  • Enhanced Electrical Properties of 3D Printed Bi2Te3-Based Thermoelectric Materials via Hot Isostatic Pressing
    Seungki Jo
    Ceramist.2025; 28(1): 126.     CrossRef
  • Hot isostatic pressing-driven fine-tuning of electrical properties in p- and n-type (Bi,Sb)2Te3 thermoelectric materials
    Seungki Jo, Jeong Min Park, Linh Ba Vu, Haeum Park, Soo Ho Jung, Jinhee Bae, Jong Min Park, Jungho Choe, Kyung Tae Kim
    Ceramics International.2025; 51(26): 51107.     CrossRef
Article image
[English]
Data-driven Approach to Explore the Contribution of Process Parameters for Laser Powder Bed Fusion of a Ti-6Al-4V Alloy
Jeong Min Park, Jaimyun Jung, Seungyeon Lee, Haeum Park, Yeon Woo Kim, Ji-Hun Yu
J Powder Mater. 2024;31(2):137-145.   Published online April 30, 2024
DOI: https://doi.org/10.4150/jpm.2024.00038
  • 3,686 View
  • 91 Download
  • 5 Citations
AbstractAbstract PDF
In order to predict the process window of laser powder bed fusion (LPBF) for printing metallic components, the calculation of volumetric energy density (VED) has been widely calculated for controlling process parameters. However, because it is assumed that the process parameters contribute equally to heat input, the VED still has limitation for predicting the process window of LPBF-processed materials. In this study, an explainable machine learning (xML) approach was adopted to predict and understand the contribution of each process parameter to defect evolution in Ti alloys in the LPBF process. Various ML models were trained, and the Shapley additive explanation method was adopted to quantify the importance of each process parameter. This study can offer effective guidelines for fine-tuning process parameters to fabricate high-quality products using LPBF.

Citations

Citations to this article as recorded by  
  • Data-Driven analysis relates mechanical properties to pore morphology in laser powder bed fusion
    Jaemin Wang, Seungyeon Lee, Yeon Woo Kim, Kyung Tae Kim, Jeong Min Park, Dierk Raabe
    Acta Materialia.2026; 304: 121751.     CrossRef
  • Effect of Support Structure on Residual Stress Distribution in Ti-6Al-4V Alloy Fabricated by Laser Powder Bed Fusion
    Seungyeon Lee, Haeum Park, Min Jae Baek, Dong Jun Lee, Jae Wung Bae, Ji-Hun Yu, Jeong Min Park
    Journal of Powder Materials.2025; 32(3): 244.     CrossRef
  • Automated segmentation and analysis of microscopy images of laser powder bed fusion melt tracks
    Aagam Shah, Reimar Weissbach, David A. Griggs, A. John Hart, Elif Ertekin, Sameh Tawfick
    Journal of Manufacturing Processes.2025; 154: 61.     CrossRef
  • Coefficient of Thermal Expansion of AlSi10Mg, 316L Stainless Steel and Ti6Al4V Alloys Made with Laser Powder Bed Fusion
    Selami Emanet, Edem Honu, Kekeli Agbewornu, Evelyn Quansah, Congyuan Zeng, Patrick Mensah
    Materials.2025; 18(19): 4468.     CrossRef
  • Adaptive slicing for increased productivity of metal laser powder bed fusion
    Lars Vanmunster, Louca R. Goossens, Laurent Sergeant, Brecht Van Hooreweder, Bey Vrancken
    Additive Manufacturing.2025; 112: 105000.     CrossRef
Special Article
Article image
[Korean]
Study on the Elemental Diffusion Distance of a Pure Nickel Layer Additively Manufactured on 316H Stainless Steel
UiJun Ko, Won Chan Lee, Gi Seung Shin, Ji-Hyun Yoon, Jeoung Han Kim
J Powder Mater. 2024;31(3):220-225.   Published online June 27, 2024
DOI: https://doi.org/10.4150/jpm.2024.00164
  • 1,332 View
  • 45 Download
  • 4 Citations
AbstractAbstract PDF
Molten salt reactors represent a promising advancement in nuclear technology due to their potential for enhanced safety, higher efficiency, and reduced nuclear waste. However, the development of structural materials that can survive under severe corrosion environments is crucial. In the present work, pure Ni was deposited on the surface of 316H stainless steel using a directed energy deposition (DED) process. This study aimed to fabricate pure Ni alloy layers on an STS316H alloy substrate. It was observed that low laser power during the deposition of pure Ni on the STS316H substrate could induce stacking defects such as surface irregularities and internal voids, which were confirmed through photographic and SEM analyses. Additionally, the diffusion of Fe and Cr elements from the STS316H substrate into the Ni layers was observed to decrease with increasing Ni deposition height. Analysis of the composition of Cr and Fe components within the Ni deposition structures allows for the prediction of properties such as the corrosion resistance of Ni.

Citations

Citations to this article as recorded by  
  • Microstructural analysis and characterization of nickel deposition on 316H stainless steel via gas tungsten arc welding and powder laser cladding
    Won Chan Lee, Jin Woong Park, Seung Ju Nam, Ji-Hyun Yoon, Jeoung Han Kim
    Powder Metallurgy.2025; 68(4): 342.     CrossRef
  • Effect of oxygen content in feedstock powders on microstructure and mechanical properties of ELI Ti-6Al-4V fabricated via laser powder bed fusion
    Woo Hyeok Kim, Sang Woo Kim, Raj Narayan Hajra, Gargi Roy, Jeoung Han Kim
    Powder Metallurgy.2025; 68(4): 307.     CrossRef
  • Development of Aluminum Alloys for Additive Manufacturing Using Machine Learning
    Sungbin An, Juyeon Han, Seoyeon Jeon, Dowon Kim, Jae Bok Seol, Hyunjoo Choi
    Journal of Powder Materials.2025; 32(3): 202.     CrossRef
  • Evaluation of Mechanical Properties of Pure Ni Coatings on a Type 316H Stainless Steel Substrate via High-Velocity Oxy-fuel and Directed Energy Deposition Processes
    Won Chan Lee, Seung Ju Nam, Ji-Hyun Yoon, Jeoung Han Kim
    Journal of Powder Materials.2025; 32(4): 309.     CrossRef
Research Article
Article image
[English]
Cryogenic Tensile Behavior of Ferrous Medium-entropy Alloy Additively Manufactured by Laser Powder Bed Fusion
Seungyeon Lee, Kyung Tae Kim, Ji-Hun Yu, Hyoung Seop Kim, Jae Wung Bae, Jeong Min Park
J Powder Mater. 2024;31(1):8-15.   Published online February 28, 2024
DOI: https://doi.org/10.4150/KPMI.2024.31.1.8
  • 3,681 View
  • 130 Download
  • 4 Citations
AbstractAbstract PDF

The emergence of ferrous-medium entropy alloys (FeMEAs) with excellent tensile properties represents a potential direction for designing alloys based on metastable engineering. In this study, an FeMEA is successfully fabricated using laser powder bed fusion (LPBF), a metal additive manufacturing technology. Tensile tests are conducted on the LPBF-processed FeMEA at room temperature and cryogenic temperatures (77 K). At 77 K, the LPBF-processed FeMEA exhibits high yield strength and excellent ultimate tensile strength through active deformation-induced martensitic transformation. Furthermore, due to the low stability of the face-centered cubic (FCC) phase of the LPBF-processed FeMEA based on nano-scale solute heterogeneity, stress-induced martensitic transformation occurs, accompanied by the appearance of a yield point phenomenon during cryogenic tensile deformation. This study elucidates the origin of the yield point phenomenon and deformation behavior of the FeMEA at 77 K.

Citations

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  • Effect of Building Orientation on Tensile Properties of Hastelloy X alloy Manufactured by Laser Powder Bed Fusion
    Seong-June Youn, GooWon Noh, Seok Su Sohn, Young-Sang Na, Young-Kyun Kim
    Journal of Powder Materials.2025; 32(2): 130.     CrossRef
  • Thermodynamic and Electronic Descriptor-Driven Machine Learning for Phase Prediction in High-Entropy Alloys: Experimental Validation
    Nguyen Lam Khoa, Nguyen Duy Khanh, Hoang Thi Ngoc Quyen, Nguyen Thi Hoang, Oanh, Le Hong Thang, Nguyen Hoa Khiem, Nguyen Hoang Viet
    Journal of Powder Materials.2025; 32(3): 191.     CrossRef
  • Cryogenic tensile behavior of carbon-doped CoCrFeMnNi high-entropy alloys additively manufactured by laser powder bed fusion
    Haeum Park, Hyeonseok Kwon, Kyung Tae Kim, Ji-Hun Yu, Jungho Choe, Hyokyung Sung, Hyoung Seop Kim, Jung Gi Kim, Jeong Min Park
    Additive Manufacturing.2024; 86: 104223.     CrossRef
  • Recent progress in high-entropy alloys for laser powder bed fusion: Design, processing, microstructure, and performance
    Asker Jarlöv, Zhiguang Zhu, Weiming Ji, Shubo Gao, Zhiheng Hu, Priyanka Vivegananthan, Yujia Tian, Devesh Raju Kripalani, Haiyang Fan, Hang Li Seet, Changjun Han, Liming Tan, Feng Liu, Mui Ling Sharon Nai, Kun Zhou
    Materials Science and Engineering: R: Reports.2024; 161: 100834.     CrossRef
Articles
Article image
[Korean]
Combinatorial Experiment for Al-6061 and Al-12Si alloy Based on Directed Energy Deposition (DED) Process
Seoyeon Jeon, Suwon Park, Yongwook Song, Jiwon Park, Hyunyoung Park, Boram Lee, Hyunjoo Choi
J Powder Mater. 2023;30(6):463-469.   Published online December 1, 2023
DOI: https://doi.org/10.4150/KPMI.2023.30.6.463
  • 1,715 View
  • 44 Download
  • 4 Citations
AbstractAbstract PDF

Aluminum alloys, known for their high strength-to-weight ratios and impressive electrical and thermal conductivities, are extensively used in numerous engineering sectors, such as aerospace, automotive, and construction. Recently, significant efforts have been made to develop novel aluminum alloys specifically tailored for additive manufacturing. These new alloys aim to provide an optimal balance between mechanical properties and thermal/ electrical conductivities. In this study, nine combinatorial samples with various alloy compositions were fabricated using direct energy deposition (DED) additive manufacturing by adjusting the feeding speeds of Al6061 alloy and Al-12Si alloy powders. The effects of the alloying elements on the microstructure, electrical conductivity, and hardness were investigated. Generally, as the Si and Cu contents decreased, electrical conductivity increased and hardness decreased, exhibiting trade-off characteristics. However, electrical conductivity and hardness showed an optimal combination when the Si content was adjusted to below 4.5 wt%, which can sufficiently suppress the grain boundary segregation of the α- Si precipitates, and the Cu content was controlled to induce the formation of Al2Cu precipitates.

Citations

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  • Development of Aluminum Alloys for Additive Manufacturing Using Machine Learning
    Sungbin An, Juyeon Han, Seoyeon Jeon, Dowon Kim, Jae Bok Seol, Hyunjoo Choi
    Journal of Powder Materials.2025; 32(3): 202.     CrossRef
  • Trends in Materials Modeling and Computation for Metal Additive Manufacturing
    Seoyeon Jeon, Hyunjoo Choi
    journal of Korean Powder Metallurgy Institute.2024; 31(3): 213.     CrossRef
  • The Challenges and Advances in Recycling/Re-Using Powder for Metal 3D Printing: A Comprehensive Review
    Alex Lanzutti, Elia Marin
    Metals.2024; 14(8): 886.     CrossRef
  • Microstructural Effects on the Mechanical Properties of Ti-6Al-4V Fabricated by Direct Energy Deposition
    Juho Kim, Seoyeon Jeon, Hwajin Park, Taeyoel Kim, Hyunjoo Choi
    Journal of Powder Materials.2024; 31(4): 302.     CrossRef
Article image
[Korean]
A Study on the Optimal Design of Ti-6Al-4V Lattice Structure Manufactured by Laser Powder Bed Fusion Process
Ji-Yoon Kim, Jeongmin Woo, Yongho Sohn, Jeong Ho Kim, Kee-Ahn Lee
J Powder Mater. 2023;30(2):146-155.   Published online April 1, 2023
DOI: https://doi.org/10.4150/KPMI.2023.30.2.146
  • 1,262 View
  • 21 Download
  • 4 Citations
AbstractAbstract PDF

The Ti-6Al-4V lattice structure is widely used in the aerospace industry owing to its high specific strength, specific stiffness, and energy absorption. The quality, performance, and surface roughness of the additively manufactured parts are significantly dependent on various process parameters. Therefore, it is important to study process parameter optimization for relative density and surface roughness control. Here, the part density and surface roughness are examined according to the hatching space, laser power, and scan rotation during laser-powder bed fusion (LPBF), and the optimal process parameters for LPBF are investigated. It has high density and low surface roughness in the specific process parameter ranges of hatching space (0.06–0.12 mm), laser power (225–325 W), and scan rotation (15°). In addition, to investigate the compressive behavior of the lattice structure, a finite element analysis is performed based on the homogenization method. Finite element analysis using the homogenization method indicates that the number of elements decreases from 437,710 to 27 and the analysis time decreases from 3,360 to 9 s. In addition, to verify the reliability of this method, stress–strain data from the compression test and analysis are compared.

Citations

Citations to this article as recorded by  
  • Effect of Support Structure on Residual Stress Distribution in Ti-6Al-4V Alloy Fabricated by Laser Powder Bed Fusion
    Seungyeon Lee, Haeum Park, Min Jae Baek, Dong Jun Lee, Jae Wung Bae, Ji-Hun Yu, Jeong Min Park
    Journal of Powder Materials.2025; 32(3): 244.     CrossRef
  • Enhanced Microstructure and Wear Resistance of Ti–6Al–4V Alloy with Vanadium Carbide Coating via Directed Energy Deposition
    Ui Jun Ko, Ju Hyeong Jung, Jung Hyun Kang, Kyunsuk Choi, Jeoung Han Kim
    Materials.2024; 17(3): 733.     CrossRef
  • Microstructural Evolution and Mechanical Properties of Ti-6Al-4V Alloy through Selective Laser Melting: Comprehensive Study on the Effect of Hot Isostatic Pressing (HIP)
    Gargi Roy, Raj Narayan Hajra, Woo Hyeok Kim, Jongwon Lee, Sangwoo Kim, Jeoung Han Kim
    journal of Korean Powder Metallurgy Institute.2024; 31(1): 1.     CrossRef
  • Data-driven Approach to Explore the Contribution of Process Parameters for Laser Powder Bed Fusion of a Ti-6Al-4V Alloy
    Jeong Min Park, Jaimyun Jung, Seungyeon Lee, Haeum Park, Yeon Woo Kim, Ji-Hun Yu
    journal of Korean Powder Metallurgy Institute.2024; 31(2): 137.     CrossRef
Article image
[Korean]
Thermoelectric Performance Enhancement of Sintered Bi-Te Pellets by Rotary-type Atomic Layer Deposition
Myeong Jun Jung, Ji Young Park, Su Min Eun, Byung Joon Choi
J Powder Mater. 2023;30(2):130-139.   Published online April 1, 2023
DOI: https://doi.org/10.4150/KPMI.2023.30.2.130
  • 1,252 View
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  • 4 Citations
AbstractAbstract PDF

Thermoelectric materials and devices are energy-harvesting devices that can effectively recycle waste heat into electricity. Thermoelectric power generation is widely used in factories, engines, and even in human bodies as they continuously generate heat. However, thermoelectric elements exhibit poor performance and low energy efficiency; research is being conducted to find new materials or improve the thermoelectric performance of existing materials, that is, by ensuring a high figure-of-merit (zT) value. For increasing zT, higher σ (electrical conductivity) and S (Seebeck coefficient) and a lower к (thermal conductivity) are required. Here, interface engineering by atomic layer deposition (ALD) is used to increase zT of n-type BiTeSe (BTS) thermoelectric powders. ALD of the BTS powders is performed in a rotary-type ALD reactor, and 40 to 100 ALD cycles of ZnO thin films are conducted at 100°C. The physical and chemical properties and thermoelectric performance of the ALD-coated BTS powders and pellets are characterized. It is revealed that electrical conductivity and thermal conductivity are decoupled, and thus, zT of ALD-coated BTS pellets is increased by more than 60% compared to that of the uncoated BTS pellets. This result can be utilized in a novel method for improving the thermoelectric efficiency in materials processing.

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  • Highly deformable and hierarchical 3D composite sponge for versatile thermoelectric energy conversion
    Jong Min Park, Changyeon Baek, Min-Ku Lee, Nagamalleswara Rao Alluri, Gyoung-Ja Lee, Kyung Tae Kim, Kwi-Il Park
    Applied Surface Science.2025; 692: 162730.     CrossRef
  • Thermal Confinement and Filtering Effect of SnSe by Insertion of Atomic-Layer-Deposited ZnO Interfacial Layer
    Myeong Jun Jung, Su Min Eun, Hogyoung Kim, Seong Keun Kim, Jongmin Byun, Byung Joon Choi
    Korean Journal of Chemical Engineering.2025;[Epub]     CrossRef
  • Investigation of the Thermal-to-Electrical Properties of Transition Metal-Sb Alloys Synthesized for Thermoelectric Applications
    Jong Min Park, Seungki Jo, Sooho Jung, Jinhee Bae, Linh Ba Vu, Kwi-Il Park, Kyung Tae Kim
    journal of Korean Powder Metallurgy Institute.2024; 31(3): 236.     CrossRef
  • Enhancing Electrical Properties of N-type Bismuth Telluride Alloys through Graphene Oxide Incorporation in Extrusion 3D Printing
    Jinhee Bae, Seungki Jo, Kyung Tae Kim
    journal of Korean Powder Metallurgy Institute.2023; 30(4): 318.     CrossRef
Article image
[Korean]
Enhancement of Thermoelectric Performance in Spark Plasma Sintered p-Type Bi0.5Sb1.5Te3.0 Compound via Hot Isostatic Pressing (HIP) Induced Reduction of Lattice Thermal Conductivity
Soo-Ho Jung, Ye Jin Woo, Kyung Tae Kim, Seungki Jo
J Powder Mater. 2023;30(2):123-129.   Published online April 1, 2023
DOI: https://doi.org/10.4150/KPMI.2023.30.2.123
  • 1,390 View
  • 8 Download
  • 4 Citations
AbstractAbstract PDF

High-temperature and high-pressure post-processing applied to sintered thermoelectric materials can create nanoscale defects, thereby enhancing their thermoelectric performance. Here, we investigate the effect of hot isostatic pressing (HIP) as a post-processing treatment on the thermoelectric properties of p-type Bi0.5Sb1.5Te3.0 compounds sintered via spark plasma sintering. The sample post-processed via HIP maintains its electronic transport properties despite the reduced microstructural texturing. Moreover, lattice thermal conductivity is significantly reduced owing to activated phonon scattering, which can be attributed to the nanoscale defects created during HIP, resulting in an ~18% increase in peak zT value, which reaches ~1.43 at 100°C. This study validates that HIP enhances the thermoelectric performance by controlling the thermal transport without having any detrimental effects on the electronic transport properties of thermoelectric materials.

Citations

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  • Enhanced Electrical Properties of 3D Printed Bi2Te3-Based Thermoelectric Materials via Hot Isostatic Pressing
    Seungki Jo
    Ceramist.2025; 28(1): 126.     CrossRef
  • Exploring Thermoelectric Transport Properties and Band Parameters of n-Type Bi2-xSbxTe3 Compounds Using the Single Parabolic Band Model
    Linh Ba Vu, Soo-ho Jung, Jinhee Bae, Jong Min Park, Kyung Tae Kim, Injoon Son, Seungki Jo
    journal of Korean Powder Metallurgy Institute.2024; 31(2): 119.     CrossRef
  • Investigation of the Thermal-to-Electrical Properties of Transition Metal-Sb Alloys Synthesized for Thermoelectric Applications
    Jong Min Park, Seungki Jo, Sooho Jung, Jinhee Bae, Linh Ba Vu, Kwi-Il Park, Kyung Tae Kim
    journal of Korean Powder Metallurgy Institute.2024; 31(3): 236.     CrossRef
  • Enhancing Electrical Properties of N-type Bismuth Telluride Alloys through Graphene Oxide Incorporation in Extrusion 3D Printing
    Jinhee Bae, Seungki Jo, Kyung Tae Kim
    journal of Korean Powder Metallurgy Institute.2023; 30(4): 318.     CrossRef
Research Articles
Article image
[English]
Ultra-Low-Temperature (4.2 K) Tensile Properties and Deformation Mechanism of Stainless Steel 304L Manufactured by Laser Powder Bed Fusion
Seung-Min Jeon, Young-Sang Na, Young-Kyun Kim
J Powder Mater. 2025;32(2):95-103.   Published online April 30, 2025
DOI: https://doi.org/10.4150/jpm.2025.00066
  • 1,247 View
  • 46 Download
  • 3 Citations
AbstractAbstract PDF
This study investigated the ultra-low-temperature (4.2 K) tensile properties and deformation mechanisms of stainless steel 304L manufactured via laser powder bed fusion (LPBF). The tensile properties of LPBF 304L were compared to those of conventional 304L to assess its suitability for cryogenic applications. The results revealed that LPBF 304L exhibited a significantly higher yield strength but lower ultimate tensile strength and elongation than conventional 304L at 4.2 K. The temperature dependence of the yield strength also favored LPBF 304L. Microstructural analysis demonstrated that LPBF 304L features a high density of dislocation cells and nano-inclusions, contributing to its greater strength. Furthermore, strain-induced martensitic transformation was observed as a key deformation mechanism at cryogenic temperatures, where austenite transformed into both hexagonal-closed packed (HCP) and body-centered cubic (BCC) martensite. Notably, BCC martensite nucleation occurred within a single HCP band. These findings provide critical insights into the mechanical behavior of LPBF 304L at cryogenic temperatures and its potential for applications in extreme environments.

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  • Extremely low-temperature tensile behavior of 316L stainless steel additively manufactured by laser powder bed fusion
    Haeum Park, Heechan Jung, Min Young Sung, Young-Kyun Kim, Jaimyun Jung, Yoona Lee, Namhyun Kang, Kyung Tae Kim, Young-Sang Na, Seok Su Sohn, Jeong Min Park
    Materials Science and Engineering: A.2026; 950: 149460.     CrossRef
  • Twinning- and transformation-induced high cryogenic strength and ductility of the CoCrFeNi high-entropy alloy: Experiment and MD simulation
    Yuze Wu, Zhide Li, Charlie Kong, M.W. Fu, Hailiang Yu
    International Journal of Plasticity.2026; 196: 104553.     CrossRef
  • Understanding the unique appearance behavior of shear bands during tensile deformation of α-brass at 4.2 K
    Seon-Keun Oh, Sang-Hun Shim, Young-Kyun Kim, Young-Sang Na
    Materials Science and Engineering: A.2025; 945: 148989.     CrossRef
Article image
[English]
A Parametric Study on the L-PBF Process of an AlSi10Mg Alloy for High-Speed Productivity of Automotive Prototype Parts
Yeonha Chang, Hyomoon Joo, Wanghyun Yong, Yeongcheol Jo, Seongjin Kim, Hanjae Kim, Yeon Woo Kim, Kyung Tae Kim, Jeong Min Park
J Powder Mater. 2024;31(5):390-398.   Published online October 31, 2024
DOI: https://doi.org/10.4150/jpm.2024.00325
  • 1,713 View
  • 50 Download
  • 3 Citations
AbstractAbstract PDF
The AlSi10Mg alloy has garnered significant attention for its application in laser powder bed fusion (L-PBF), due to its lightweight properties and good printability using L-PBF. However, the low production speed of the L-PBF process is the main bottleneck in the industrial commercialization of L-PBF AlSi10Mg alloy parts. Furthermore, while L-PBF AlSi10Mg alloy exhibits excellent mechanical properties, the properties are often over-specified compared to the target properties of parts traditionally fabricated by casting. To accelerate production speed in L-PBF, this study investigated the effects of process parameters on the build rate and mechanical properties of the AlSi10Mg alloy. Guidelines are proposed for high-speed additive manufacturing of the AlSi10Mg alloy for use in automotive parts. The results show a significant increase in the build rate, exceeding the conventional build rate by a factor of 3.6 times or more, while the L-PBF AlSi10Mg alloy met the specifications for automotive prototype parts. This strategy can be expected to offer significant cost advantages while maintaining acceptable mechanical properties of topology-optimized parts used in the automobile industry.

Citations

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  • Lightweight Design of a Connecting Rod Using Lattice-Structure Parameter Optimisation: A Test Case for L-PBF
    Michele Amicarelli, Michele Trovato, Paolo Cicconi
    Machines.2025; 13(3): 171.     CrossRef
  • Effect of Support Structure on Residual Stress Distribution in Ti-6Al-4V Alloy Fabricated by Laser Powder Bed Fusion
    Seungyeon Lee, Haeum Park, Min Jae Baek, Dong Jun Lee, Jae Wung Bae, Ji-Hun Yu, Jeong Min Park
    Journal of Powder Materials.2025; 32(3): 244.     CrossRef
  • Data-Driven Analysis relates Mechanical Properties to Pore Morphology in Laser Powder Bed Fusion
    Jaemin Wang, Seungyeon Lee, Yeon Woo Kim, Kyung Tae Kim, Jeong Min Park, Dierk Raabe
    Acta Materialia.2025; : 121751.     CrossRef
Critical Review
Article image
[English]
A Review of Inorganic Solid Electrolytes for All-Solid-State Lithium Batteries: Challenges and Progress
Seul Ki Choi, Jaehun Han, Gi Jeong Kim, Yeon Hee Kim, Jaewon Choi, MinHo Yang
J Powder Mater. 2024;31(4):293-301.   Published online August 30, 2024
DOI: https://doi.org/10.4150/jpm.2024.00206
  • 8,322 View
  • 200 Download
  • 3 Citations
AbstractAbstract PDF
All-solid-state lithium batteries (ASSLBs) are receiving attention as a prospective next-generation secondary battery technology that can reduce the risk of commercial lithium-ion batteries by replacing flammable organic liquid electrolytes with non-flammable solid electrolytes. The practical application of ASSLBs requires developing robust solid electrolytes that possess ionic conductivity at room temperature on a par with that of organic liquids. These solid electrolytes must also be thermally and chemically stable, as well as compatible with electrode materials. Inorganic solid electrolytes, including oxide and sulfide-based compounds, are being studied as promising future candidates for ASSLBs due to their higher ionic conductivity and thermal stability than polymer electrolytes. Here, we present the challenges currently facing the development of oxide and sulfide-based solid electrolytes, as well as the research efforts underway aiming to resolve these challenges.

Citations

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  • A facile synthesis of bulk LiPON in solution for solid-state electrolytes
    Osma J. Gomez, Adam Antar, Alex T. Hall, Leopoldo Tapia-Aracayo, Joshua Seo, Nam Kim, Zihan Sun, Ryan Lim, Fu Chen, Yue Li, John Cumings, Gary Rubloff, Sang Bok Lee, David Stewart, Yang Wang
    Journal of Materials Chemistry A.2025; 13(34): 28368.     CrossRef
  • Uniform lithium deposition using Cu teepee structures for anode-free lithium metal batteries
    Seo Yun Jung, Jaehun Han, Seul Ki Choi, Se Youn Cho, Jong Ho Won, Jaewon Choi, Minho Yang
    Chemical Engineering Journal.2025; 522: 167302.     CrossRef
  • Garnet-type LLZO electrolytes for solid-state lithium batteries: Interfaces, conductivity, in-situ processing, and industrial prospects
    Kaleab Habtamu Ayalew, Nithyadharseni Palaniyandy, Mkhulu K. Mathe, Phumlani F. Msomi
    Chemical Engineering Journal.2025; 524: 168098.     CrossRef
Review Paper
Article image
[English]
Research Trends in Electromagnetic Shielding using MXene-based Composite Materials
Siyeon Kim, Jongmin Byun
J Powder Mater. 2024;31(1):57-76.   Published online February 28, 2024
DOI: https://doi.org/10.4150/KPMI.2024.31.1.57
  • 6,523 View
  • 145 Download
  • 3 Citations
AbstractAbstract PDF

Recent advancements in electronic devices and wireless communication technologies, particularly the rise of 5G, have raised concerns about the escalating electromagnetic pollution and its potential adverse impacts on human health and electronics. As a result, the demand for effective electromagnetic interference (EMI) shielding materials has grown significantly. Traditional materials face limitations in providing optimal solutions owing to inadequacy and low performance due to small thickness. MXene-based composite materials have emerged as promising candidates in this context owing to their exceptional electrical properties, high conductivity, and superior EMI shielding efficiency across a broad frequency range. This review examines the recent developments and advantages of MXene-based composite materials in EMI shielding applications, emphasizing their potential to address the challenges posed by electromagnetic pollution and to foster advancements in modern electronics systems and vital technologies.

Citations

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  • Designing dual phase hexaferrite (SrFe12O19) – Perovskite (La0.5Nd0.5FeO3) composites for enhanced electromagnetic wave absorption and band gap modulation
    Pramod D. Mhase, Varsha C. Pujari, Santosh S. Jadhav, Abdullah G. Al-Sehemi, Sarah Alsobaie, Sunil M. Patange
    Composites Communications.2025; 54: 102284.     CrossRef
  • Microstructure tailoring of Nb-based MAX phase by low temperature synthesis with layer-structured Nb2C powder and molten salt method
    Chaehyun Lim, Wonjune Choi, Jongmin Byun
    Materials Characterization.2025; 225: 115106.     CrossRef
  • Fabrication of MOF@MXene composites via surface modification of MXene under acidic conditions
    Ji-Haeng Jeong, Woong-Ryeol Yu
    Functional Composites and Structures.2025; 7(2): 025006.     CrossRef
Articles
Article image
[Korean]
Exploration of Aluminum Alloy using Multi-feeder 3D Additive Manufacturing-based Combinatorial Experiment
Suwon Park, Yongwook Song, Jiyoon Yeo, Songyun Han, Hyunjoo Choi
J Powder Mater. 2023;30(3):255-261.   Published online June 1, 2023
DOI: https://doi.org/10.4150/KPMI.2023.30.3.255
  • 1,375 View
  • 8 Download
  • 3 Citations
AbstractAbstract PDF

Aluminum alloys are widely utilized in diverse industries, such as automobiles, aerospace, and architecture, owing to their high specific strength and resistance to oxidation. However, to meet the increasing demands of the industry, it is necessary to design new aluminum alloys with excellent properties. Thus, a new method is required to efficiently test additively manufactured aluminum alloys with various compositions within a short period during the alloy design process. In this study, a combinatory approach using a direct energy deposition system for metal 3D printing process with a dual feeder was employed. Two types of aluminum alloy powders, namely Al6061 and Al-12Cu, were utilized for the combinatory test conducted through 3D printing. Twelve types of Al-Si-Cu-Mg alloys were manufactured during this combinatory test, and the relationship between their microstructures and properties was investigated.

Citations

Citations to this article as recorded by  
  • Trends in Materials Modeling and Computation for Metal Additive Manufacturing
    Seoyeon Jeon, Hyunjoo Choi
    journal of Korean Powder Metallurgy Institute.2024; 31(3): 213.     CrossRef
  • Microstructural Effects on the Mechanical Properties of Ti-6Al-4V Fabricated by Direct Energy Deposition
    Juho Kim, Seoyeon Jeon, Hwajin Park, Taeyoel Kim, Hyunjoo Choi
    Journal of Powder Materials.2024; 31(4): 302.     CrossRef
  • Combinatorial Experiment for Al-6061 and Al-12Si alloy Based on Directed Energy Deposition (DED) Process
    Seoyeon Jeon, Suwon Park, Yongwook Song, Jiwon Park, Hyunyoung Park, Boram Lee, Hyunjoo Choi
    journal of Korean Powder Metallurgy Institute.2023; 30(6): 463.     CrossRef
Article image
[English]
Fabrication of Equiatomic CoCrFeMnNi High-Entropy Alloy by Metal Injection Molding Process Using Coarse-Sized Powders
Eun Seong Kim, Jae Man Park, Ji Sun Lee, Jungho Choe, Soung Yeoul Ahn, Sang Guk Jeong, Do Won Lee, Seong Jin Park, Hyoung Seop Kim
J Powder Mater. 2023;30(1):1-6.   Published online February 1, 2023
DOI: https://doi.org/10.4150/KPMI.2023.30.1.1
  • 1,413 View
  • 32 Download
  • 3 Citations
AbstractAbstract PDF

High-entropy alloys (HEAs) are attracting attention because of their excellent properties and functions; however, they are relatively expensive compared with commercial alloys. Therefore, various efforts have been made to reduce the cost of raw materials. In this study, MIM is attempted using coarse equiatomic CoCrFeMnNi HEA powders. The mixing ratio (powder:binder) for HEA feedstock preparation is explored using torque rheometer. The block-shaped green parts are fabricated through a metal injection molding process using feedstock. The thermal debinding conditions are explored by thermogravimetric analysis, and solvent and thermal debinding are performed. It is densified under various sintering conditions considering the melting point of the HEA. The final product, which contains a small amount of non-FCC phase, is manufactured at a sintering temperature of 1250°C.

Citations

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  • Development of 3D interconnected nanoporous TiZrHfNbTaNi high-entropy alloy via liquid metal dealloying and subsequent synthesis of (TiZrHfNbTaNi)O high-entropy oxide
    Jae Hyuk Lee, Soo Vin Ha, Jihye Seong, Akira Takeuchi, Ruirui Song, Hidemi Kato, Soo-Hyun Joo
    Journal of Materials Research and Technology.2025; 35: 5204.     CrossRef
  • Development of 3D interconnected heterogeneous high-entropy alloy composites with enhanced multifunctionality via liquid metal dealloying
    Munsu Choi, Gang Hee Gu, Jongun Moon, Jae Wung Bae, Hidemi Kato, Seung Zeon Han, Hyoung Seop Kim, Yongseok Choi, Soo-Hyun Joo
    Journal of Materials Research and Technology.2025; 37: 5672.     CrossRef
  • Characterization of the Manufacturing Process and Mechanical Properties of CoCrFeMnNi High-Entropy Alloys via Metal Injection Molding and Hot Isostatic Pressing
    Eun Seong Kim, Jae Man Park, Do Won Lee, Hyojeong Ha, Jungho Choe, Jaemin Wang, Seong Jin Park, Byeong-Joo Lee, Hyoung Seop Kim
    journal of Korean Powder Metallurgy Institute.2024; 31(3): 243.     CrossRef
Research Article
Article image
[English]
Thermodynamic and Electronic Descriptor-Driven Machine Learning for Phase Prediction in High-Entropy Alloys: Experimental Validation
Nguyen Lam Khoa, Nguyen Duy Khanh, Hoang Thi Ngoc Quyen, Nguyen Thi Hoang Oanh, , Le Hong Thang, Nguyen Hoa Khiem, Nguyen Hoang Viet
J Powder Mater. 2025;32(3):191-201.   Published online June 30, 2025
DOI: https://doi.org/10.4150/jpm.2025.00143
  • 1,486 View
  • 63 Download
  • 2 Citations
AbstractAbstract PDF
High-entropy alloys (HEAs) exhibit complex phase formation behavior, challenging conventional predictive methods. This study presents a machine learning (ML) framework for phase prediction in HEAs, using a curated dataset of 648 experimentally characterized compositions and features derived from thermodynamic and electronic descriptors. Three classifiers—random forest, gradient boosting, and CatBoost—were trained and validated through cross-validation and testing. Gradient boosting achieved the highest accuracy, and valence electron concentration (VEC), atomic size mismatch (δ), and enthalpy of mixing (ΔHmix) were identified as the most influential features. The model predictions were experimentally verified using a non-equiatomic Al₃₀Cu₁₇.₅Fe₁₇.₅Cr₁₇.₅Mn₁₇.₅ alloy and the equiatomic Cantor alloy (CoCrFeMnNi), both of which showed strong agreement with predicted phase structures. The results demonstrate that combining physically informed feature engineering with ML enables accurate and generalizable phase prediction, supporting accelerated HEA design.

Citations

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  • Preparation and Arc Erosion Behavior of Cu-Based Contact Materials Reinforced with High Entropy Particles CuCrNiCoFe
    Jiacheng Tong, Jun Wang, Huimin Zhang, Haoran Liu, Youchang Sun, Zhiguo Li, Wenyi Zhang, Zhe Wang, Yanli Chang, Zhao Yuan, Henry Hu
    Metallurgical and Materials Transactions B.2025; 56(5): 5948.     CrossRef
  • Recent progresses on high entropy alloy development using machine learning: A review
    Abhishek Kumar, Nilay Krishna Mukhopadhyay, Thakur Prasad Yadav
    Computational Materials Today.2025; 8: 100038.     CrossRef
Critical Reviews
Article image
[English]
Advances in Powder Metallurgy for High-Entropy Alloys
Sheetal Kumar Dewangan, Cheenepalli Nagarjuna, Hansung Lee, K. Raja Rao, Man Mohan, Reliance Jain, Byungmin Ahn
J Powder Mater. 2024;31(6):480-492.   Published online December 31, 2024
DOI: https://doi.org/10.4150/jpm.2024.00297
  • 3,601 View
  • 136 Download
  • 2 Citations
AbstractAbstract PDF
High-entropy alloys (HEAs) represent a revolutionary class of materials characterized by their multi-principal element compositions and exceptional mechanical properties. Powder metallurgy, a versatile and cost-effective manufacturing process, offers significant advantages for the development of HEAs, including precise control over their composition, microstructure, and mechanical properties. This review explores innovative approaches integrating powder metallurgy techniques in the synthesis and optimization of HEAs. Key advances in powder production, sintering methods, and additive manufacturing are examined, highlighting their roles in improving the performance, advancement, and applicability of HEAs. The review also discusses the mechanical properties, potential industrial applications, and future trends in the field, providing a comprehensive overview of the current state and future prospects of HEA development using powder metallurgy.

Citations

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  • Fabrication and Alloying Behavior of Ultra-Lightweight AlTiCrVMg High-Entropy Alloy via Al-Mg Mutual Solubility and Sintering Control
    Eunhyo Song, Hansung Lee, Byungmin Ahn
    Journal of Powder Materials.2025; 32(3): 254.     CrossRef
  • Thermodynamic and Electronic Descriptor-Driven Machine Learning for Phase Prediction in High-Entropy Alloys: Experimental Validation
    Nguyen Lam Khoa, Nguyen Duy Khanh, Hoang Thi Ngoc Quyen, Nguyen Thi Hoang, Oanh, Le Hong Thang, Nguyen Hoa Khiem, Nguyen Hoang Viet
    Journal of Powder Materials.2025; 32(3): 191.     CrossRef
Article image
[English]
Comparative Review of the Microstructural and Mechanical Properties of Ti-6Al-4V Fabricated via Wrought and Powder Metallurgy Processes
Raj Narayan Hajra, Gargi Roy, An Seong Min, Hyunseok Lee, Jeoung Han Kim
J Powder Mater. 2024;31(5):365-373.   Published online October 31, 2024
DOI: https://doi.org/10.4150/jpm.2024.00213
  • 1,970 View
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  • 2 Citations
AbstractAbstract PDF
This review examines the microstructural and mechanical properties of a Ti-6Al-4V alloy produced by wrought processing and powder metallurgy (PM), specifically laser powder bed fusion (LPBF) and hot isostatic pressing. Wrought methods, such as forging and rolling, create equiaxed alpha (α) and beta (β) grain structures with balanced properties, which are ideal for fatigue resistance. In contrast, PM methods, particularly LPBF, often yield a martensitic α′ structure with high microhardness, enabling complex geometries but requiring post-processing to improve its properties and reduce stress. The study evaluated the effects of processing parameters on grain size, phase distribution, and material characteristics, guiding the choice of fabrication techniques for optimizing Ti-6Al-4V performance in aerospace, biomedical, and automotive applications. The analysis emphasizes tailored processing to meet advanced engineering demands.

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  • Removal of Organic and Inorganic Contaminants from Titanium Turning Scrap via Alkali and Acid Two-Step Cleaning
    Seong Min An, Raj Narayan Hajra, Chan Hee Park, Jin-Ho Yoon, Jinsung Rho, Chang-Min Yoon, Jeoung Han Kim
    MATERIALS TRANSACTIONS.2025; 66(7): 855.     CrossRef
  • Effect of oxygen content in feedstock powders on microstructure and mechanical properties of ELI Ti-6Al-4V fabricated via laser powder bed fusion
    Woo Hyeok Kim, Sang Woo Kim, Raj Narayan Hajra, Gargi Roy, Jeoung Han Kim
    Powder Metallurgy.2025; 68(4): 307.     CrossRef
Research Articles
Article image
[Korean]
Effect of Sintering Conditions on the Microstructure of an FeCrMnNiCo High-Entropy Alloy
Seonghyun Park, Sang-Hwa Lee, Junho Lee, Seok-Jae Lee, Jae-Gil Jung
J Powder Mater. 2024;31(5):406-413.   Published online October 31, 2024
DOI: https://doi.org/10.4150/jpm.2024.00185
  • 1,019 View
  • 30 Download
  • 2 Citations
AbstractAbstract PDF
We investigated the microstructure of an FeCrMnNiCo alloy fabricated by spark plasma sintering under different sintering temperatures (1000–1100°C) and times (1–600 s). All sintered alloys consisted of a single face-centered cubic phase. As the sintering time or temperature increased, the grains of the sintered alloys became partially coarse. The formation of Cr7C3 carbide occurred on the surface of the sintered alloys due to carbon diffusion from the graphite crucible. The depth of the layer containing Cr7C3 carbides increased to ~110 μm under severe sintering conditions (1100°C, 60 s). A molten zone was observed on the surface of the alloys sintered at higher temperatures (>1060°C) due to severe carbon diffusion that reduced the melting point of the alloy. The porosity of the sintered alloys decreased with increasing time at 1000°C, but increased at higher temperatures above 1060°C due to melting-induced porosity formation.

Citations

Citations to this article as recorded by  
  • Fabrication and Alloying Behavior of Ultra-Lightweight AlTiCrVMg High-Entropy Alloy via Al-Mg Mutual Solubility and Sintering Control
    Eunhyo Song, Hansung Lee, Byungmin Ahn
    Journal of Powder Materials.2025; 32(3): 254.     CrossRef
  • Microstructure and mechanical properties of oxide-dispersion-strengthened CrMnFeCoNiC0.2O0.2 high-entropy alloy fabricated by mechanical alloying and spark plasma sintering
    Sang-Hwa Lee, Seonghyun Park, Ka Ram Lim, Seok-Jae Lee, Jae-Gil Jung
    Materials Science and Engineering: A.2025; 947: 149284.     CrossRef
Article image
[Korean]
Effect of Anisotropy on the Wear Behavior of Age-Treated Maraging Steel Manufactured by LPBF
Seung On Lim, Se-Eun Shin
J Powder Mater. 2024;31(4):308-317.   Published online August 5, 2024
DOI: https://doi.org/10.4150/jpm.2024.00171
  • 1,733 View
  • 33 Download
  • 2 Citations
AbstractAbstract PDF
Maraging steel has excellent mechanical properties resulting from the formation of precipitates within the matrix through aging treatment. Maraging steel fabricated by the laser powder bed fusion (LPBF) process is suitable for applications including precise components and optimized design. The anisotropic characteristic, which depends on the stacking direction, affects the mechanical properties. This study aimed to analyze the influence of anisotropy on the wear behavior of maraging steel after aging treatment. The features of additive manufacturing tended to disappear after heat treatment. However, some residual cellular and dendrite structures were observed. In the wear tests, a high wear rate was observed on the building direction plane for all counter materials. This is believed to be because the oxides formed on the wear track positively affected the wear characteristics; meanwhile, the bead shape in the stacking direction surface was vulnerable to wear, leading to significant wear.

Citations

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  • Unveiling age-hardening mechanisms: first-principles carbide insights and enhanced thermomechanical fatigue in niobium-bearing austenitic stainless steels
    Godwin Kwame Ahiale, Jin Woong Park, Raj Narayan Hajra, Yong-Jun Oh, Won Doo Choi, Tae-Wook Na, Gi Yong Kim, Hyun-Ju Choi, Jeoung Han Kim
    Materials Science and Engineering: A.2026; 949: 149397.     CrossRef
  • A Parametric Study on the L-PBF Process of an AlSi10Mg Alloy for High-Speed Productivity of Automotive Prototype Parts
    Yeonha Chang, Hyomoon Joo, Wanghyun Yong, Yeongcheol Jo, Seongjin Kim, Hanjae Kim, Yeon Woo Kim, Kyung Tae Kim, Jeong Min Park
    Journal of Powder Materials.2024; 31(5): 390.     CrossRef
Special Article
Article image
[English]
Trends in Materials Modeling and Computation for Metal Additive Manufacturing
Seoyeon Jeon, Hyunjoo Choi
J Powder Mater. 2024;31(3):213-219.   Published online June 27, 2024
DOI: https://doi.org/10.4150/jpm.2024.00150
  • 2,039 View
  • 67 Download
  • 2 Citations
AbstractAbstract PDF
Additive Manufacturing (AM) is a process that fabricates products by manufacturing materials according to a three-dimensional model. It has recently gained attention due to its environmental advantages, including reduced energy consumption and high material utilization rates. However, controlling defects such as melting issues and residual stress, which can occur during metal additive manufacturing, poses a challenge. The trial-and-error verification of these defects is both time-consuming and costly. Consequently, efforts have been made to develop phenomenological models that understand the influence of process variables on defects, and mechanical/electrical/thermal properties of geometrically complex products. This paper introduces modeling techniques that can simulate the powder additive manufacturing process. The focus is on representative metal additive manufacturing processes such as Powder Bed Fusion (PBF), Direct Energy Deposition (DED), and Binder Jetting (BJ) method. To calculate thermal-stress history and the resulting deformations, modeling techniques based on Finite Element Method (FEM) are generally utilized. For simulating the movements and packing behavior of powders during powder classification, modeling techniques based on Discrete Element Method (DEM) are employed. Additionally, to simulate sintering and microstructural changes, techniques such as Monte Carlo (MC), Molecular Dynamics (MD), and Phase Field Modeling (PFM) are predominantly used.

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  • Review of “Integrated Computer-Aided Process Engineering Session in the 17th International Symposium on Novel and Nano Materials (ISNNM, 14–18 November 2022)”
    Yeon-Joo Lee, Pil-Ryung Cha, Hyoung-Seop Kim, Hyun-Joo Choi
    MATERIALS TRANSACTIONS.2025; 66(1): 144.     CrossRef
  • Effect of Support Structure on Residual Stress Distribution in Ti-6Al-4V Alloy Fabricated by Laser Powder Bed Fusion
    Seungyeon Lee, Haeum Park, Min Jae Baek, Dong Jun Lee, Jae Wung Bae, Ji-Hun Yu, Jeong Min Park
    Journal of Powder Materials.2025; 32(3): 244.     CrossRef
Research Articles
Article image
[English]
Investigation of the Thermal-to-Electrical Properties of Transition Metal-Sb Alloys Synthesized for Thermoelectric Applications
Jong Min Park, Seungki Jo, Sooho Jung, Jinhee Bae, Linh Ba Vu, Kwi-Il Park, Kyung Tae Kim
J Powder Mater. 2024;31(3):236-242.   Published online June 27, 2024
DOI: https://doi.org/10.4150/jpm.2024.00031
  • 1,375 View
  • 43 Download
  • 2 Citations
AbstractAbstract PDF
The development of thermoelectric (TE) materials to replace Bi2Te3 alloys is emerging as a hot issue with the potential for wider practical applications. In particular, layered Zintl-phase materials, which can appropriately control carrier and phonon transport behaviors, are being considered as promising candidates. However, limited data have been reported on the thermoelectric properties of metal-Sb materials that can be transformed into layered materials through the insertion of cations. In this study, we synthesized FeSb and MnSb, which are used as base materials for advanced thermoelectric materials. They were confirmed as single-phase materials by analyzing X-ray diffraction patterns. Based on electrical conductivity, the Seebeck coefficient, and thermal conductivity of both materials characterized as a function of temperature, the zT values of MnSb and FeSb were calculated to be 0.00119 and 0.00026, respectively. These properties provide a fundamental data for developing layered Zintl-phase materials with alkali/alkaline earth metal insertions.

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  • Improving thermoelectric properties of CuMnSb alloys via strategic alloying with magnetic MnSb and Cu
    Jong Min Park, Seungki Jo, Soo-ho Jung, Jinhee Bae, Linh Ba Vu, Jihun Yu, Kyung Tae Kim
    Materials Letters.2025; 381: 137796.     CrossRef
  • Highly deformable and hierarchical 3D composite sponge for versatile thermoelectric energy conversion
    Jong Min Park, Changyeon Baek, Min-Ku Lee, Nagamalleswara Rao Alluri, Gyoung-Ja Lee, Kyung Tae Kim, Kwi-Il Park
    Applied Surface Science.2025; 692: 162730.     CrossRef
Article image
[Korean]
Effect of Abnormal Grain Growth on Ionic Conductivity in LATP
Hyungik Choi, Yoonsoo Han
J Powder Mater. 2024;31(1):23-29.   Published online February 28, 2024
DOI: https://doi.org/10.4150/KPMI.2024.31.1.23
  • 2,470 View
  • 62 Download
  • 2 Citations
PDF

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  • Temperature-dependent microstructural evolution in a compositionally complex solid electrolyte: The role of a grain boundary transition
    Shu-Ting Ko, Chaojie Du, Huiming Guo, Hasti Vahidi, Jenna L. Wardini, Tom Lee, Yi Liu, Jingjing Yang, Francisco Guzman, Timothy J. Rupert, William J. Bowman, Shen J. Dillon, Xiaoqing Pan, Jian Luo
    Journal of Advanced Ceramics.2025; 14(3): 9221047.     CrossRef
  • Effect of bimodal particle size distribution on Li1.5Al0.5Ti1.5(PO4)3 solid electrolytes: Microstructures and electrochemical properties
    Gi Jeong Kim, Yeon Hee Kim, Seul Ki Choi, Jong Won Bae, Kun-Jae Lee, Minho Yang
    Powder Technology.2025; 466: 121407.     CrossRef
Review Paper
Article image
[English]
Eco-Friendly Powder and Particles-Based Triboelectric Energy Harvesters
Rayyan Ali Shaukat, Jihun Choi, Chang Kyu Jeong
J Powder Mater. 2023;30(6):528-535.   Published online December 1, 2023
DOI: https://doi.org/10.4150/KPMI.2023.30.6.528
  • 1,634 View
  • 35 Download
  • 2 Citations
AbstractAbstract PDF

Since their initial development in 2012, triboelectric nanogenerators (TENGs) have gained popularity worldwide as a desired option for harnessing energy. The urgent demand for TENGs is attributed to their novel structural design, low cost, and use of large-scale materials. The output performance of a TENG depends on the surface charge density of the friction layers. Several recycled and biowaste materials have been explored as friction layers to enhance the output performance of TENGs. Natural and oceanic biomaterials have also been investigated as alternatives for improving the performance of TENG devices. Moreover, structural innovations have been made in TENGs to develop highly efficient devices. This review summarizes the recent developments in recycling and biowaste materials for TENG devices. The potential of natural and oceanic biowaste materials is also discussed. Finally, future outlooks for the structural developments in TENG devices are presented.

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  • Fabrication and Characterization of a Flexible Polyurethane-Based Triboelectric Nanogenerator for a Harvesting Energy System
    Saba Ejaz, Imran Shah, Shahid Aziz, Gul Hassan, Ahmed Shuja, Muhammad Asif Khan, Dong-Won Jung
    Micromachines.2025; 16(2): 230.     CrossRef
  • Optimized Process and Mechanical and Electrical Analysis of Polyimide/Pb(Zr,Ti)O3-Based Flexible Piezoelectric Composites
    Junki Lee, Sang-il Yoon, Hyunseung Kim, Chang Kyu Jeong
    Journal of Powder Materials.2025; 32(1): 16.     CrossRef
Articles
Article image
[Korean]
Fabrication of Flexible Energy Harvester Based on BaTiO3 Piezoelectric Nanotube Arrays
Seo Young Yoon, Cheol Min Kim, Bitna Bae, Yujin Na, Haksu Jang, Kwi-Il Park
J Powder Mater. 2023;30(6):521-527.   Published online December 1, 2023
DOI: https://doi.org/10.4150/KPMI.2023.30.6.521
  • 802 View
  • 15 Download
  • 2 Citations
AbstractAbstract PDF

Piezoelectric technology, which converts mechanical energy into electrical energy, has recently attracted drawn considerable attention in the industry. Among the many kinds of piezoelectric materials, BaTiO3 nanotube arrays, which have outstanding uniformity and anisotropic orientation compared to nanowire-based arrays, can be fabricated using a simple synthesis process. In this study, we developed a flexible piezoelectric energy harvester (f-PEH) based on a composite film with PVDF-coated BaTiO3 nanotube arrays through sequential anodization and hydrothermal synthesis processes. The f-PEH fabricated using the piezoelectric composite film exhibited excellent piezoelectric performance and high flexibility compared to the previously reported BaTiO3 nanotube array-based energy harvester. These results demonstrate the possibility for widely application with high performance by our advanced f-PEH technique based on BaTiO3 nanotube arrays.

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  • Flexible Thermoelectric Energy Harvester with Stacked Structure of Thermoelectric Composite Films Made of PVDF and Bi2Te3-Based Particles
    Da Eun Shin, Nagamalleswara Rao Alluri, Kwi-Il Park
    ACS Applied Energy Materials.2024; 7(19): 8288.     CrossRef
  • CoFe2O4-BaTiO3 core-shell-embedded flexible polymer composite as an efficient magnetoelectric energy harvester
    Bitna Bae, Nagamalleswara Rao Alluri, Cheol Min Kim, Jungho Ryu, Gwang Hyeon Kim, Hyeon Jun Park, Changyeon Baek, Min-Ku Lee, Gyoung-Ja Lee, Geon-Tae Hwang, Kwi-Il Park
    Materials Today Physics.2024; 48: 101567.     CrossRef
Article image
[Korean]
Thermal Stability and Weight Reduction of Al0.75V2.82CrZr Refractory High Entropy Alloy Prepared Via Mechanical Alloying
Minsu Kim, Hansung Lee, Byungmin Ahn
J Powder Mater. 2023;30(6):478-483.   Published online December 1, 2023
DOI: https://doi.org/10.4150/KPMI.2023.30.6.478
  • 964 View
  • 15 Download
  • 2 Citations
AbstractAbstract PDF

High-entropy alloys (HEAs) are characterized by having five or more main elements and forming simple solids without forming intermetallic compounds, owing to the high entropy effect. HEAs with these characteristics are being researched as structural materials for extreme environments. Conventional refractory alloys have excellent hightemperature strength and stability; however, problems occur when they are used extensively in a high-temperature environment, leading to reduced fatigue properties due to oxidation or a limited service life. In contrast, refractory entropy alloys, which provide refractory properties to entropy alloys, can address these issues and improve the hightemperature stability of the alloy through phase control when designed based on existing refractory alloy elements. Refractory high-entropy alloys require sufficient milling time while in the process of mechanical alloying because of the brittleness of the added elements. Consequently, the high-energy milling process must be optimized because of the possibility of contamination of the alloyed powder during prolonged milling. In this study, we investigated the hightemperature oxidation behavior of refractory high-entropy alloys while optimizing the milling time.

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  • Tailored high-temperature oxidation behavior and nanomechanical properties of Al0.75VCrZrNb lightweight refractory high-entropy alloys
    Hansung Lee, Hwi Geun Yu, Reliance Jain, Man Mohan, Younggeon Lee, Sheetal Kumar Dewangan, Byungmin Ahn
    International Journal of Refractory Metals and Hard Materials.2026; 135: 107507.     CrossRef
  • Simultaneous enhancement of strength and ductility of Al matrix composites enabled by submicron-sized high-entropy alloy phases
    Chahee Jung, Seungin Nam, Hansol Son, Juyeon Han, Jaewon Jeong, Hyokyung Sung, Hyoung Seop Kim, Seok Su Sohn, Hyunjoo Choi
    Journal of Materials Research and Technology.2024; 33: 1470.     CrossRef
Article image
[Korean]
Epoxy-Based Siloxane/Silica Composites for Electronic Packaging by Composition and Molecular Structure of Siloxane, and Analysis of Changes in Properties
Junho Jang, Dong Jun Kang, Hyeon-Gyun Im
J Powder Mater. 2023;30(4):346-355.   Published online August 1, 2023
DOI: https://doi.org/10.4150/KPMI.2023.30.4.346
  • 941 View
  • 10 Download
  • 2 Citations
AbstractAbstract PDF

Epoxy-based composites find extensive application in electronic packaging due to their excellent processability and insulation properties. However, conventional epoxy-based polymers exhibit limitations in terms of thermal properties and insulation performance. In this study, we develop epoxy-based siloxane/silica composites that enhance the thermal, mechanical, and insulating properties of epoxy resins. This is achieved by employing a sol–gelsynthesized siloxane hybrid and spherical fused silica particles. Herein, we fabricate two types of epoxy-based siloxane/ silica composites with different siloxane molecular structures (branched and linear siloxane networks) and investigate the changes in their properties for different compositions (with or without silica particles) and siloxane structures. The presence of a branched siloxane structure results in hardness and low insulating properties, while a linear siloxane structure yields softness and highly insulating properties. Both types of epoxy-based siloxane/silica composites exhibit high thermal stability and low thermal expansion. These properties are considerably improved by incorporating silica particles. We expect that our developed epoxy-based composites to hold significant potential as advanced electronic packaging materials, offering high-performance and robustness.

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  • Toughening epoxy matrices via elastomeric blending for enhanced compatibility with auxetic reinforcements in composites
    Usama Khalid, Shiza Shahid, Muhammad Bilal Qadir, Mumtaz Ali, Zubair Khaliq, Aamir Naseem Satti, Zaheer Anwar Randhawa, Danish Umer
    Mechanics Based Design of Structures and Machines.2025; : 1.     CrossRef
  • Enhanced Epoxy Composites Reinforced by 3D-Aligned Aluminum Borate Nanowhiskers
    Hyunseung Song, Kiho Song, Haejin Hwang, Changui Ahn
    Materials.2024; 17(19): 4727.     CrossRef
Article image
[Korean]
Effect of Substrate Pre-heating on Microstructure and Magnetic Properties of Nd-Fe-B Permanent Magnet Manufactured by L-PBF
Yeon Woo Kim, Haeum Park, Tae-Hoon Kim, Kyung Tae Kim, Ji-Hun Yu, Yoon Suk Choi, Jeong Min Park
J Powder Mater. 2023;30(2):116-122.   Published online April 1, 2023
DOI: https://doi.org/10.4150/KPMI.2023.30.2.116
  • 896 View
  • 14 Download
  • 2 Citations
AbstractAbstract PDF

Because magnets fabricated using Nd-Fe-B exhibit excellent magnetic properties, this novel material is used in various high-tech industries. However, because of the brittleness and low formability of Nd-Fe-B magnets, the design freedom of shapes for improving the performance is limited based on conventional tooling and postprocessing. Laserpowder bed fusion (L-PBF), the most famous additive manufacturing (AM) technique, has recently emerged as a novel process for producing geometrically complex shapes of Nd-Fe-B parts owing to its high precision and good spatial resolution. However, because of the repeated thermal shock applied to the materials during L-PBF, it is difficult to fabricate a dense Nd-Fe-B magnet. In this study, a high-density (>96%) Nd-Fe-B magnet is successfully fabricated by minimizing the thermal residual stress caused by substrate heating during L-PBF.

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  • Effect of Support Structure on Residual Stress Distribution in Ti-6Al-4V Alloy Fabricated by Laser Powder Bed Fusion
    Seungyeon Lee, Haeum Park, Min Jae Baek, Dong Jun Lee, Jae Wung Bae, Ji-Hun Yu, Jeong Min Park
    Journal of Powder Materials.2025; 32(3): 244.     CrossRef
  • Linkage between process-induced microstructure and magnetic property of Nd-Fe-B permanent magnets additively manufactured by laser powder bed fusion
    Yeon Woo Kim, Sujin Lee, Yoona Lee, Jae Bok Seol, Namhyun Kang, Yoon Suk Choi, Ji-Hun Yu, Jung-Goo Lee, Tae-Hoon Kim, Jeong Min Park
    Materials & Design.2025; 259: 114929.     CrossRef
Article image
[Korean]
Changes in Mechanical and Electrical Properties as a Function of Unidirectional Pressure Changes in Preforming While Isostatic Pressing for Graphite Block Fabrication
Tae-Sub Byun, Dong-Pyo Jeon, Sang-Hye Lee, Sang-Woo Lee, Jae-Seung Roh
J Powder Mater. 2023;30(1):35-40.   Published online February 1, 2023
DOI: https://doi.org/10.4150/KPMI.2023.30.1.35
  • 1,412 View
  • 9 Download
  • 2 Citations
AbstractAbstract PDF

In this study, a graphite block is fabricated using artificial graphite processing byproduct and phenolic resin as raw materials. Mechanical and electrical property changes are confirmed due to the preforming method. After fabricating preforms at 50, 100, and 150 MPa, CIP molding at 150 MPa is followed by heat treatment to prepare a graphite block. 150UP-CIP shows a 12.9% reduction in porosity compared with the 150 MPa preform. As the porosity is decreased, the bulk density, flexural strength, and shore hardness are increased by 14.9%, 102.4%, and 13.7%, respectively; and the deviation of density and electrical resistivity are decreased by 51.9% and 34.1%, respectively. Therefore, as the preforming pressure increases, the porosity decreases, and the electrical and mechanical properties improve.

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  • Effect of Microstructural Change under Pressure during Isostatic Pressing on Mechanical and Electrical Properties of Isotropic Carbon Blocks
    Tae-Sub Byun, Sang-Hye Lee, Suk-Hwan Kim, Jae-Seung Roh
    Materials.2024; 17(2): 387.     CrossRef
  • Effect of Pressure and Holding Time during Compression Molding on Mechanical Properties and Microstructure of Coke-Pitch Carbon Blocks
    Sun-Ung Gwon, Sang-Hye Lee, U-Sang Youn, Jae-Seung Roh
    Applied Sciences.2024; 14(2): 772.     CrossRef
Article image
[English]
Investigation on Microstructure and Flowability of Gas Atomized Heat-resistant KHR45A Alloy Powders for Additive Manufacturing
Geonwoo Baek, Mohsen Saboktakin Rizi, Yeeun Lee, SungJae Jo, Joo-Hyun Choi, Soon-Jik Hong
J Powder Mater. 2023;30(1):13-21.   Published online February 1, 2023
DOI: https://doi.org/10.4150/KPMI.2023.30.1.13
  • 2,166 View
  • 766 Download
  • 2 Citations
AbstractAbstract PDF

In additive manufacturing, the flowability of feedstock particles determines the quality of the parts that are affected by different parameters, including the chemistry and morphology of the powders and particle size distribution. In this study, the microstructures and flowabilities of gas-atomized heat-resistant alloys for additive manufacturing applications are investigated. A KHR45A alloy powder with a composition of Fe-30Cr-40Mn-1.8Nb (wt.%) is fabricated using gas atomization process. The microstructure and effect of powder chemistry and morphology on the flow behavior are investigated by scanning electron microscopy (SEM), X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), and revolution powder analysis. The results reveal the formation of spherical particles composed of single-phase FCC dendritic structures after gas atomization. SEM observations show variations in the microstructures of the powder particles with different size distributions. Elemental distribution maps, line scans, and high-resolution XPS results indicate the presence of a Si-rich oxide accompanied by Fe, Cr, and Nb metal oxides in the outer layer of the powders. The flowability behavior is found to be induced by the particle size distribution, which can be attributed to the interparticle interactions and friction of particles with different sizes.

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  • Engineering heterogeneous microstructure for enhancing mechanical properties of multicomponent alloys via powder metallurgy route
    Min Woo Shin, Sung-Jae Jo, Sourabh Kumar Soni, Ji-Woon Lee, Jongun Moon, Hyoung Seop Kim, Soon-Jik Hong
    Materials Science and Engineering: A.2025; 941: 148599.     CrossRef
  • Al-based amorphous coatings by warm spraying: Numerical simulation and experimental validation
    Deming Wang, Nianchu Wu, Peng Cao
    Journal of Alloys and Compounds.2024; 1008: 176674.     CrossRef
Research Article
Article image
[Korean]
Extraction of MgSO4 from dolomite and synthesis of Mg(OH)2 in Bittern
HyunSeung Shim, Jiyeon Kim, Areum Choi, Nuri Oh, YooJin Kim
J Powder Mater. 2025;32(2):122-130.   Published online April 30, 2025
DOI: https://doi.org/10.4150/jpm.2025.00073
  • 691 View
  • 29 Download
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AbstractAbstract PDF
We synthesized magnesium hydroxide using bittern and dolomite, which are domestic resources. In Bittern, there is a high concentration of Mg2+ ions, but the impurity Ca2+ ion content is also significant, requiring a purification process to remove it. There are two main methods for this purification. Firstly, there is a separation method that utilizes the difference in solubility between Mg2+ ions and Ca2+ ions by using sulfuric acid on dolomite. Adding MgSO4 solution from dolomite to Bittern removes Ca2+ ions as CaSO4. This process simultaneously purifies Ca impurities and increases the Mg/Ca ratio by adding extra Mg2+ ions. In this study, purified bittern was obtained by using dolomite and sulfuric acid to extract MgSO4, which was then used to purify Ca2+ ions. High-purity Mg(OH)2 was synthesized by optimizing the NaOH and NH4OH ratio as an alkaline precipitant.

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  • Synthesis and Morphology Control of Needle Type 513 MHSH and Mg(OH)2 from Dolomite
    Jiyeon Kim, HyunSeung Shim, Seong-Ju Hwang, YooJin Kim
    Journal of Powder Materials.2025; 32(5): 399.     CrossRef
Critical Review
Article image
[English]
A Review of Recent Developments in CoCrFeMnNi High-Entropy Alloys Processed by Powder Metallurgy
Cheenepalli Nagarjuna, Sheetal Kumar Dewangan, Hansung Lee, Eunhyo Song, K. Raja Rao, Byungmin Ahn
J Powder Mater. 2025;32(2):145-164.   Published online April 30, 2025
DOI: https://doi.org/10.4150/jpm.2024.00430
  • 3,165 View
  • 86 Download
  • 1 Citations
AbstractAbstract PDF
In recent years, high-entropy alloys (HEAs) have attracted considerable attention in materials engineering due to their unique phase stability and mechanical properties compared to conventional alloys. Since the inception of HEAs, CoCrFeMnNi alloys have been widely investigated due to their outstanding strength and fracture toughness at cryogenic temperatures. However, their lower yield strength at room temperature limits their structural applications. The mechanical properties of HEAs are greatly influenced by their processing methods and microstructural features. Unlike traditional melting techniques, powder metallurgy (PM) provides a unique opportunity to produce HEAs with nanocrystalline structures and uniform compositions. The current review explores recent advances in optimizing the microstructural characteristics in CoCrFeMnNi HEAs by using PM techniques to improve mechanical performance. The most promising strategies include grain refinement, dispersion strengthening, and the development of heterogeneous microstructures (e.g., harmonic, bimodal, and multi-metal lamellar structures). Thermomechanical treatments along with additive manufacturing techniques are also summarized. Additionally, the review addresses current challenges and suggests future research directions for designing advanced HEAs through PM techniques.

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  • Thermodynamic and Electronic Descriptor-Driven Machine Learning for Phase Prediction in High-Entropy Alloys: Experimental Validation
    Nguyen Lam Khoa, Nguyen Duy Khanh, Hoang Thi Ngoc Quyen, Nguyen Thi Hoang, Oanh, Le Hong Thang, Nguyen Hoa Khiem, Nguyen Hoang Viet
    Journal of Powder Materials.2025; 32(3): 191.     CrossRef
Research Article
Article image
[Korean]
Effect of Hatch Spacing on the Microstructure and Mechanical Properties of SA508 Gr.3 Steel Fabricated by Laser Powder Bed Fusion
Yuanjiu Huang, Ho Jin Ryu, Kee-Ahn Lee
J Powder Mater. 2025;32(1):50-58.   Published online February 28, 2025
DOI: https://doi.org/10.4150/jpm.2024.00479
  • 869 View
  • 20 Download
  • 1 Citations
AbstractAbstract PDF
This study investigated the effect of the hatch spacing parameter on the microstructure and mechanical properties of SA508 Gr.3 steel manufactured by laser powder bed fusion (L-PBF) for a nuclear pressure vessel. Materials were prepared with varying hatch spacing (0.04 mm [H4] and 0.06 mm [H6]). The H4 exhibited finer and more uniformly distributed grains, while the H6 showed less porosity and a lower defect fraction. The yield strength of the H4 material was higher than that of the H6 material, but there was a smaller difference between the materials in tensile strength. The measured elongation was 5.65% for the H4 material and 10.41% for the H6 material, showing a significantly higher value for H6. An explanation for this is that although the H4 material had a microstructure of small and uniform grains, it contained larger and more numerous pore defects than the H6 material, facilitating stress concentration and the initiation of microcracks.

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  • Extremely low temperature mechanical behavior of in-situ oxide containing 304L stainless steel fabricated by laser powder bed fusion
    Kwangtae Son, Seung-Min Jeon, Brian K. Paul, Young-Sang Na, Kijoon Lee, Young-Kyun Kim
    Journal of Materials Science & Technology.2025; 234: 319.     CrossRef
Critical Review
Article image
[English]
Recent Advances in Thermoelectric Materials and Devices: Improving Power Generation Performance
Momanyi Amos Okirigiti, Cheol Min Kim, Hyejeong Choi, Nagamalleswara Rao Alluri, Kwi-Il Park
J Powder Mater. 2025;32(1):1-15.   Published online February 28, 2025
DOI: https://doi.org/10.4150/jpm.2024.00395
  • 7,495 View
  • 176 Download
  • 1 Citations
AbstractAbstract PDF
Thermoelectric materials have been the focus of extensive research interest in recent years due to their potential in clean power generation from waste heat. Their conversion efficiency is primarily reflected by the dimensionless figure of merit, with higher values indicating better performance. There is a pressing need to discover materials that increase output power and improve performance, from the material level to device fabrication. This review provides a comprehensive analysis of recent advancements, such as Bi2Te3-based nanostructures that reduce thermal conductivity while maintaining electrical conductivity, GeTe-based high entropy alloys that utilize multiple elements for improved thermoelectric properties, porous metal-organic frameworks offering tunable structures, and organic/hybrid films that present low-cost, flexible solutions. Innovations in thermoelectric generator designs, such as asymmetrical geometries, segmented modules, and flexible devices, have further contributed to increased efficiency and output power. Together, these developments are paving the way for more effective thermoelectric technologies in sustainable energy generation.

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  • Mathematical and simulation modeling of photovoltaic systems utilizing thermoelectric modules for effective thermal management
    Muhammad Sohaib Tahir, Xue Dong, Muhammad Mansoor Khan
    Results in Engineering.2025; 27: 106344.     CrossRef
Research Article
Article image
[English]
Design of Conductive Inks Containing Carbon Black and Silver Nanowires for Patternable Screen-Printing on Fabrics
Seokhwan Kim, Geumseong Lee, Jinwoo Park, Dahye Shin, Ki-Il Park, Kyoung Jin Jung, Yuho Min
J Powder Mater. 2024;31(6):500-507.   Published online December 31, 2024
DOI: https://doi.org/10.4150/jpm.2024.00409
  • 1,628 View
  • 46 Download
  • 1 Citations
AbstractAbstract PDF
This study developed conductive inks composed of carbon black (CB) and silver nanowires (Ag NWs) for cost-effective screen-printing on fabrics. The Ag NW density within the CB matrix was precisely controlled, achieving tunable electrical conductivity with minimal Ag NW usage. The resulting inks were successfully patterned into shapes such as square grids and circles on textile surfaces, demonstrating excellent conductivity and fidelity. Adding 19.9 wt% Ag NWs reduced sheet resistance by ~92% compared to CB-only inks, highlighting the effectiveness and potential of this hybrid approach for cost-effective, high-performance textile-based electronics. The one-dimensional morphology of Ag NWs facilitated the formation of conductive percolation networks, creating efficient electron pathways within the CB matrix even at low loadings. This work advances the field of CB-based conductive inks and provides a scalable and practical method for producing functional, patterned electronic textiles.

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  • Multifunctional Screen-Printed Conductive Inks: Design Principles, Performance Challenges, and Application Horizons
    Nahid Islam, Manisha Das, Bashir Ahmed Johan, Syed Shaheen Shah, Atif Saeed Alzahrani, Md. Abdul Aziz
    ACS Applied Electronic Materials.2025; 7(16): 7503.     CrossRef
Critical Review
Article image
[English]
Epsilon Iron Oxide (ε-Fe2O3) as an Electromagnetic Functional Material: Properties, Synthesis, and Applications
Ji Hyeong Jeong, Hwan Hee Kim, Jung-Goo Lee, Youn-Kyoung Baek
J Powder Mater. 2024;31(6):465-479.   Published online December 31, 2024
DOI: https://doi.org/10.4150/jpm.2024.00290
  • 2,425 View
  • 76 Download
  • 1 Citations
AbstractAbstract PDF
Iron oxide (ε-Fe₂O₃) is emerging as a promising electromagnetic material due to its unique magnetic and electronic properties. This review focuses on the intrinsic properties of ε-Fe₂O₃, particularly its high coercivity, comparable to that of rare-earth magnets, which is attributed to its significant magnetic anisotropy. These properties render it highly suitable for applications in millimeter wave absorption and high-density magnetic storage media. Furthermore, its semiconducting behavior offers potential applications in photocatalytic hydrogen production. The review also explores various synthesis methods for fabricating ε-Fe₂O₃ as nanoparticles or thin films, emphasizing the optimization of purity and stability. By exploring and harnessing the properties of ε-Fe₂O₃, this study aims to contribute to the advancement of next-generation electromagnetic materials with potential applications in 6G wireless telecommunications, spintronics, high-density data storage, and energy technologies.

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  • Superparamagnetism of Baked Clays Containing Polymorphs of Iron Oxides: Experimental Study and Theoretical Modeling
    Petr Kharitonskii, Andrei Krasilin, Nadezhda Belskaya, Svetlana Yanson, Nikita Bobrov, Andrey Ralin, Kamil Gareev, Nikita Zolotov, Dmitry Zaytsev, Elena Sergienko
    Magnetochemistry.2025; 11(12): 103.     CrossRef
Research Articles
Article image
[English]
Hot-Cracking Behaviors in (CoNi)85Mo15 Medium-Entropy Alloys Manufactured via Powder Bed Fusion
Seungjin Nam, Heechan Jung, Haeum Park, Chahee Jung, Jeong Min Park, Hyoung Seop Kim, Seok Su Sohn
J Powder Mater. 2024;31(6):537-545.   Published online December 31, 2024
DOI: https://doi.org/10.4150/jpm.2024.00262
  • 1,072 View
  • 24 Download
  • 1 Citations
AbstractAbstract PDF
Additive manufacturing makes it possible to improve the mechanical properties of alloys through segregation engineering of specific alloying elements into the dislocation cell structure. In this study, we investigated the mechanical and microstructural characteristics of CoNi-based medium-entropy alloys (MEAs), including the refractory alloying element Mo with a large atomic radius, manufactured via laser-powder bed fusion (L-PBF). In an analysis of the printability depending on the processing parameters, we achieved a high compressive yield strength up to 653 MPa in L-PBF for (CoNi)85Mo15 MEAs. However, severe residual stress remained at high-angle grain boundaries, and a brittle µ phase was precipitated at Mo-segregated dislocation cells. These resulted in hot-cracking behaviors in (CoNi)85Mo15 MEAs during L-PBF. These findings highlight the need for further research to adjust the Mo content and processing techniques to mitigate cracking behaviors in L-PBF-manufactured (CoNi)85Mo15 MEAs.

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  • Effect of Support Structure on Residual Stress Distribution in Ti-6Al-4V Alloy Fabricated by Laser Powder Bed Fusion
    Seungyeon Lee, Haeum Park, Min Jae Baek, Dong Jun Lee, Jae Wung Bae, Ji-Hun Yu, Jeong Min Park
    Journal of Powder Materials.2025; 32(3): 244.     CrossRef
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[Korean]
Characterization of Compacted and Pressureless Sintered Parts for Molybdenum Oxide Powder according to Hydrogen Reduction Temperature
Jong Hoon Lee, Kun-Jae Lee
J Powder Mater. 2024;31(4):336-341.   Published online August 30, 2024
DOI: https://doi.org/10.4150/jpm.2024.00241
  • 958 View
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AbstractAbstract PDF
Molybdenum, valued for its high melting point and exceptional physical and chemical properties, is studied in diverse fields such as electronics, petrochemicals, and aviation. Among molybdenum oxides, molybdenum dioxide stands out for its higher electrical conductivity than other transition metal oxides due to its structural characteristics, exhibiting metallic properties. It is applied as pellets to gas sensors, semiconductors, and secondary batteries for its properties. Thus, research on molybdenum dioxide compaction and pressureless sintering is necessary, yet research on pressureless sintering is currently insufficient. This study synthesized MoO₃ powder via solution combustion synthesis and reduced it using the 3% hydrogen/argon gas mixture to investigate the effect of reduction temperature on the powder. Additionally, the reduced powder was compacted and subjected to pressureless sintering with temperature as a variable. The density and the microstructure of brown parts were analyzed and discussed.

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  • High-sensitivity optical fiber hydrogen sensing with MoO3/PANI/Pd nanocomposite
    Mohammed M. Alkhabet, Saad H. Girei, Ammar H. Farhan, Fatimah F. Hashim, Jaafar A. Jaafar, Husam K. Salih, Manar F. Abbood, Mohd H. Yaacob
    Materials Science in Semiconductor Processing.2025; 200: 110021.     CrossRef
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[Korean]
Microstructural Effects on the Mechanical Properties of Ti-6Al-4V Fabricated by Direct Energy Deposition
Juho Kim, Seoyeon Jeon, Hwajin Park, Taeyoel Kim, Hyunjoo Choi
J Powder Mater. 2024;31(4):302-307.   Published online August 30, 2024
DOI: https://doi.org/10.4150/jpm.2024.00157
  • 1,282 View
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  • 1 Citations
AbstractAbstract PDF
This study explored the process-structure-property (PSP) relationships in Ti-6Al-4V alloys fabricated through direct energy deposition (DED) additive manufacturing. A systematic investigation was conducted to clarify how process variables—specifically, manipulating the cooling rate and energy input by adjusting the laser power and scan speed during the DED process—influenced the phase fractions, pore structures, and the resultant mechanical properties of the samples under various processing conditions. Significant links were found between the controlled process parameters and the structural and mechanical characteristics of the produced alloys. The findings of this research provide foundational knowledge that will drive the development of more effective and precise control strategies in additive manufacturing, thereby improving the performance and reliability of produced materials. This, in turn, promises to make significant contributions to both the advancement of additive manufacturing technologies and their applications in critical sectors.

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  • Development of Aluminum Alloys for Additive Manufacturing Using Machine Learning
    Sungbin An, Juyeon Han, Seoyeon Jeon, Dowon Kim, Jae Bok Seol, Hyunjoo Choi
    Journal of Powder Materials.2025; 32(3): 202.     CrossRef
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[English]
Bandgap Tuning and Quenching Effects of In(Zn)P@ZnSe@ZnS Quantum Dots
Sang Yeon Lee, Su Hyun Park, Gyungsu Byun, Chang-Yeoul Kim
J Powder Mater. 2024;31(3):226-235.   Published online June 27, 2024
DOI: https://doi.org/10.4150/jpm.2024.00003
  • 2,378 View
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AbstractAbstract PDF
InP quantum dot (QDs) have attracted researchers’ interest due to their applicability in quantum dot light-emitting displays (QLED) or biomarkers for detecting cancers or viruses. The surface or interface control of InP QD core/shell has substantially increased quantum efficiency, with a quantum yield of 100% reached by introducing HF to inhibit oxide generation. In this study, we focused on the control of bandgap energy of quantum dots by changing the Zn/(In+Zn) ratio in the In(Zn)P core. Zinc incorporation can change the photoluminescent light colors of green, yellow, orange, and red. Diluting a solution of as-synthesized QDs by more than 100 times did not show any quenching effects by the Förster resonance energy transfer phenomenon between neighboring QDs.

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  • Enhancing luminescence of QD thin films, polymer composite films, and LED devices by nanostructures
    Hongcheng Yang, Junjie Hao, Mingyu Sun, Yujie Song, Kai Wang, Yujie Song, Xiao Wei Sun, Wenda Zhang
    The Innovation.2025; : 101121.     CrossRef
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[Korean]
Effect of Hot Isostatic Pressing on the Stellite 6 Alloy prepared by Directed Energy Deposition
Joowon Suh, Jae Hyeon Koh, Young-Bum Chun, Young Do Kim, Jinsung Jang, Suk Hoon Kang, Heung Nam Han
J Powder Mater. 2024;31(2):152-162.   Published online April 30, 2024
DOI: https://doi.org/10.4150/jpm.2024.00066
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AbstractAbstract PDF
The directed energy deposited (DED) alloys show higher hardness values than the welded alloys due to the finer microstructure following the high cooling rate. However, defects such as microcracks, pores, and the residual stress are remained within the DED alloy. These defects deteriorate the wear behavior so post-processing such as heat treatment and hot isostatic pressing (HIP) are applied to DED alloys to reduce the defects. HIP was chosen in this study because the high pressure and temperature uniformly reduced the defects. The HIP is processed at 1150oC under 100 MPa for 4 hours. After HIP, microcracks are disappeared and porosity is reduced by 86.9%. Carbides are spherodized due to the interdiffusion of Cr and C between the dendrite and interdendrite region. After HIP, the nanohardness (GPa) of carbides increased from 11.1 to 12, and the Co matrix decreased from 8.8 to 7.9. Vickers hardness (HV) decreased by 18.9 % after HIP. The dislocation density (10-2/m2) decreased from 7.34 to 0.34 and the residual stress (MPa) changed from tensile 79 to a compressive -246 by HIP. This study indicates that HIP is effective in reducing defects, and the HIP DED Stellite 6 exhibits a higher HV than welded Stellite 6.

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  • The Recycling Process and Powderization Technology of Stellite 6 Scrap: A Thermodynamic and Heat Transfer Analysis
    YongKwan Lee, Hyun-chul Kim, Myungsuk Kim, Soong Ju Oh, Kyoungtae Park, JaeJin Sim
    Journal of Powder Materials.2025; 32(4): 330.     CrossRef
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[Korean]
Hydrogen Reduction Behavior of NCM-based Lithium-ion Battery Cathode Materials
So-Yeong Lee, So-Yeon Lee, Dae-Hyeon Lee, Ho-Sang Sohn
J Powder Mater. 2024;31(2):163-168.   Published online April 30, 2024
DOI: https://doi.org/10.4150/jpm.2024.00017
  • 1,257 View
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AbstractAbstract PDF
As the demand for lithium-ion batteries for electric vehicles is increasing, it is important to recover valuable metals from waste lithium-ion batteries. In this study, the effects of gas flow rate and hydrogen partial pressure on hydrogen reduction of NCM-based lithium-ion battery cathode materials were investigated. As the gas flow rate and hydrogen partial pressure increased, the weight loss rate increased significantly from the beginning of the reaction due to the reduction of NiO and CoO by hydrogen. At 700 °C and hydrogen partial pressure above 0.5 atm, Ni and Li2O were produced by hydrogen reduction. From the reduction product and Li recovery rate, the hydrogen reduction of NCM-based cathode materials was significantly affected by hydrogen partial pressure. The Li compounds recovered from the solution after water leaching of the reduction products were LiOH, LiOH·H2O, and Li2CO3, with about 0.02 wt% Al as an impurity.

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  • Reduction Roasting of Black Mass Recovered from NCM-based Spent Lithium-ion Batteries Using CH4 Gas
    Sang-Yeop Lee, Jae-Ho Hwang, Ho-Sang Sohn
    Resources Recycling.2025; 34(5): 93.     CrossRef
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[Korean]
Effect of Ball Milling Conditions on the Microstructure and Dehydrogenation Behavior of TiH2 Powder
Ji Young Kim, Eui Seon Lee, Ji Won Choi, Youngmin Kim, Sung-Tag Oh
J Powder Mater. 2024;31(2):132-136.   Published online April 30, 2024
DOI: https://doi.org/10.4150/jpm.2024.00001
  • 1,805 View
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AbstractAbstract PDF
This study investigated the effects of revolution speed and ball size in planetary milling on the microstructure and dehydrogenation behavior of TiH2 powder. The particle size analysis showed that the large particles present in the raw powder were effectively refined as the revolution speed increased, and when milled at 500 rpm, the median particle size was 1.47 m. Milling with a mixture of balls of two or three sizes was more effective in refining the raw powder than milling with balls of a single size. A mixture of 3-mm and 5-mm-diameter balls was the optimal condition for particle refinement, and the measured median particle size was 0.71 m. The dependence of particle size on revolution speed and ball size was explained by changes in input energy and the number of contact points of the balls. In the milled powder, the endothermic peak measured using differential thermal analysis was observed at a relatively low temperature. This finding was interpreted as the activation of a dehydrogenation reaction, mainly due to the increase in the specific surface area and the concentration of lattice defects.

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  • Preparation and Microstructural Characteristics of Ti Nanopowder by Ball Milling and Dehydrogenation of TiH2 Powder
    Ji Young Kim, Eui Seon Lee, Ji Won Choi, Youngmin Kim, Sung-Tag Oh
    Journal of Powder Materials.2024; 31(4): 324.     CrossRef
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[Korean]
Effect of Tool Shape and Insertion Depth on Joining Properties in Friction Stir Spot Welding of Aluminum Alloy/high-strength Steel Sheets
Su-Ho An, Young-Keun Jeong
J Powder Mater. 2024;31(1):37-42.   Published online February 28, 2024
DOI: https://doi.org/10.4150/KPMI.2024.31.1.37
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  • 21 Download
  • 1 Citations
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  • Friction Welding of Casted SCM440 and Sintered F-05-140 Dissimilar Steels and Their Joint Properties under Various Welding Conditions
    Jisung Lee, Hansung Lee, Eunhyo Song, Byungmin Ahn
    Journal of Powder Materials.2024; 31(5): 414.     CrossRef
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[Korean]
Development of High-strength, High-temperature Nb-Si-Ti Alloys through Mechanical Alloying
Jung-Joon Kim, Sang-Min Yoon, Deok-Hyun Han, Jongmin Byun, Young-Kyun Kim
J Powder Mater. 2024;31(1):30-36.   Published online February 28, 2024
DOI: https://doi.org/10.4150/KPMI.2024.31.1.30
  • 1,770 View
  • 47 Download
  • 1 Citations
PDF

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  • Review of “Integrated Computer-Aided Process Engineering Session in the 17th International Symposium on Novel and Nano Materials (ISNNM, 14–18 November 2022)”
    Yeon-Joo Lee, Pil-Ryung Cha, Hyoung-Seop Kim, Hyun-Joo Choi
    MATERIALS TRANSACTIONS.2025; 66(1): 144.     CrossRef
Articles
Article image
[Korean]
Fabrication of Nanowire by Electrospinning Process Using Nickel Oxide Particle Recovered from MLCC
Haein Shin, Jongwon Bae, Minsu Kang, Kun-Jae Lee
J Powder Mater. 2023;30(6):502-508.   Published online December 1, 2023
DOI: https://doi.org/10.4150/KPMI.2023.30.6.502
  • 567 View
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AbstractAbstract PDF

With the increasing demand for electronic products, the amount of multilayer ceramic capacitor (MLCC) waste has also increased. Recycling technology has recently gained attention because it can simultaneously address raw material supply and waste disposal issues. However, research on recovering valuable metals from MLCCs and converting the recovered metals into high-value-added materials remains insufficient. Herein, we describe an electrospinning (E-spinning) process to recover nickel from MLCCs and modulate the morphology of the recovered nickel oxide particles. The nickel oxalate powder was recovered using organic acid leaching and precipitation. Nickel oxide nanoparticles were prepared via heat treatment and ultrasonic milling. A mixture of nickel oxide particles and polyvinylpyrrolidone (PVP) was used as the E-spinning solution. A PVP/NiO nanowire composite was fabricated via Espinning, and a nickel oxide nanowire with a network structure was manufactured through calcination. The nanowire diameters and morphologies are discussed based on the nickel oxide content in the E-spinning solution.

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  • Morphological Control and Surface Modification Characteristics of Nickel Oxalate Synthesized via Oxalic Acid Precipitation
    Eunbi Park, Jongwon Bae, Sera Kang, Minsu Kang, Suseong Lee, Kun-Jae Lee
    Journal of Powder Materials.2025; 32(5): 375.     CrossRef
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[Korean]
Effect of Heat Treatment on Microstructure and Mechanical Properties of Al–Zn–Mg–Cu–Si Sintered Alloys with and Without High-energy Ball Milling
Junho Lee, Seonghyun Park, Sang-Hwa Lee, Seung Bae Son, Seok-Jae Lee, Jae-Gil Jung
J Powder Mater. 2023;30(6):470-477.   Published online December 1, 2023
DOI: https://doi.org/10.4150/KPMI.2023.30.6.470
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AbstractAbstract PDF

The effects of annealing on the microstructure and mechanical properties of Al–Zn–Mg–Cu–Si alloys fabricated by high-energy ball milling (HEBM) and spark plasma sintering (SPS) were investigated. The HEBM-free sintered alloy primarily contained Mg2Si, Q-AlCuMgSi, and Si phases. Meanwhile, the HEBM-sintered alloy contains Mg-free Si and θ-Al2Cu phases due to the formation of MgO, which causes Mg depletion in the Al matrix. Annealing without and with HEBM at 500°C causes partial dissolution and coarsening of the Q-AlCuMgSi and Mg2Si phases in the alloy and dissolution of the θ-Al2Cu phase in the alloy, respectively. In both alloys, a thermally stable α-AlFeSi phase was formed after long-term heat treatment. The grain size of the sintered alloys with and without HEBM increased from 0.5 to 1.0 μm and from 2.9 to 6.3 μm, respectively. The hardness of the sintered alloy increases after annealing for 1 h but decreases significantly after 24 h of annealing. Extending the annealing time to 168 h improved the hardness of the alloy without HEBM but had little effect on the alloy with HEBM. The relationship between the microstructural factors and the hardness of the sintered and annealed alloys is discussed.

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  • Microstructural evolution and thermal stability of Al–Zn–Mg–Cu–Si–Zr alloy fabricated via spark plasma sintering
    Junho Lee, Seonghyun Park, Sang-Hwa Lee, Seung Bae Son, Hanjung Kwon, Seok-Jae Lee, Jae-Gil Jung
    Journal of Materials Research and Technology.2024; 31: 205.     CrossRef
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[Korean]
Irradiation Hardening Property of Inconel 718 Alloy produced by Selective Laser Melting
Joowon Suh, Sangyeob Lim, Hyung-Ha Jin, Young-Bum Chun, Suk Hoon Kang, Heung Nam Han
J Powder Mater. 2023;30(5):431-435.   Published online October 1, 2023
DOI: https://doi.org/10.4150/KPMI.2023.30.5.431
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An irradiation hardening of Inconel 718 produced by selective laser melting (SLM) was studied based on the microstructural observation and mechanical behavior. Ion irradiation for emulating neutron irradiation has been proposed owing to advantages such as low radiation emission and short experimental periods. To prevent softening caused by the dissolution of γ' and γ'' precipitates due to irradiation, only solution annealing (SA) was performed. SLM SA Inconel 718 specimen was ion irradiated to demonstrate the difference in microstructure and mechanical properties between the irradiated and non-irradiated specimens. After exposing specimens to Fe3+ ions irradiation up to 100 dpa (displacement per atom) at an ambient temperature, the hardness of irradiated specimens was measured by nanoindentation as a function of depth. The depth distribution profile of Fe3+ and dpa were calculated by the Monte Carlo SRIM (Stopping and Range of Ions in Matter)-2013 code under the assumption of the displacement threshold energy of 40 eV. A transmission electron microscope was utilized to observe the formation of irradiation defects such as dislocation loops. This study reveals that the Frank partial dislocation loops induce irradiation hardening of SLM SA Inconel 718 specimens.

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  • A Parametric Study on the L-PBF Process of an AlSi10Mg Alloy for High-Speed Productivity of Automotive Prototype Parts
    Yeonha Chang, Hyomoon Joo, Wanghyun Yong, Yeongcheol Jo, Seongjin Kim, Hanjae Kim, Yeon Woo Kim, Kyung Tae Kim, Jeong Min Park
    Journal of Powder Materials.2024; 31(5): 390.     CrossRef

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