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[Korean]
3D-Printed Stretchable Electrodes Enabled by a Titanium/Acrylamide-Based Hydrogel Nanocomposite
Se Jin Choi, Han Eol Lee
J Powder Mater. 2025;32(1):67-72.   Published online February 28, 2025
DOI: https://doi.org/10.4150/jpm.2024.00465
  • 267 View
  • 9 Download
AbstractAbstract PDF
Wearable electronics have been the focus of considerable interest in various fields, such as human-machine interfaces, soft robotics, and medical treatments, due to their flexibility, stretchability, and light weight. To address the shortcomings of existing metal thin film-based wearable devices, stretchable conductive polymers have been developed. In particular, double networking hydrogels are being actively studied as a polymer with a three-dimensional stereoscopic structure that can be patterned. Nonetheless, they have shortcomings such as poor electrical properties and cumbersome manufacturing processes, making it difficult to apply them in electronic devices. Herein, we report 3D-printed stretchable electrodes enabled by a titanium/polyacrylamide-alginate-based hydrogel nanocomposite. This research suggests the strategy for resolving the challenges of high costs and complex fabrication processes associated with stretchable electrode, providing a solution to accelerate the commercialization of wearable electronic devices.
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[Korean]
Optimized Process and Mechanical and Electrical Analysis of Polyimide/Pb(Zr,Ti)O3-Based Flexible Piezoelectric Composites
Junki Lee, Sang-il Yoon, Hyunseung Kim, Chang Kyu Jeong
J Powder Mater. 2025;32(1):16-22.   Published online February 28, 2025
DOI: https://doi.org/10.4150/jpm.2024.00444
  • 365 View
  • 25 Download
AbstractAbstract PDF
Piezoelectric composites have attracted significant research interest as sustainable power sources for electronic devices due to their high mechanical stability and electrical output characteristics. This study investigated the optimal processing conditions for fabricating a flexible piezoelectric energy harvester based on Pb(Zr,Ti)O₃ (PZT) powder and a polyimide (PI) matrix composite. Various parameters, including the optimal mixing ratio of PI/PZT, ultrasonic treatment, homogenization, vacuum oven, and UV/O₃ treatment, were optimized to achieve a uniform piezoelectric composite. A PZT content of 30 wt% and 20 minutes of homogenization were identified as the most effective conditions for increasing the uniformity of the composite. The optimized composite exhibited a high piezoelectric coefficient, a typical P-E hysteresis loop, and dielectric properties, exhibiting a voltage output that adjusts in response to variations in the applied touch force. This study provides foundational data for the uniform fabrication of flexible piezoelectric energy harvesters and next-generation miniaturized electronic devices.
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[Korean]
Fabrication of SiCf/SiC Composites with a BN Interphase Prepared by the Wet Method
Kyung Ho Kim, Yoonsoo Han
J Powder Mater. 2024;31(6):530-536.   Published online December 31, 2024
DOI: https://doi.org/10.4150/jpm.2024.00339
  • 319 View
  • 10 Download
AbstractAbstract PDF
This study presents a cost-effective wet chemical coating process for fabricating a boron nitride (BN) interphase on silicon carbide (SiC) fibers, increasing the oxidation resistance and performance of SiCf/SiC ceramic matrix composites. Using urea as a precursor, optimal nitriding conditions were determined by adjusting the composition, concentration, and immersion time. X-ray diffraction analysis revealed distinct BN phase formation at 1300°C and 1500°C, while a mixture of BN and B₂O₃ was observed at 1200°C. HF treatment improved coating uniformity by removing SiO₂ layers formed during the de-sizing process. Optimization of the boric acid-to-urea molar ratio resulted in a uniform, 130-nm-thick BN layer. This study demonstrates that the wet coating process offers a viable and economical alternative to chemical vapor deposition for fabricating high-performance BN interphases in SiCf/SiC composites that are suitable for high-temperature applications.
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[Korean]
Inter-laminar Strength of NITE-SiC/SiC Composites With Various Fiber Reinforcing Architecture
Jong-il Kim
J Powder Mater. 2024;31(5):437-444.   Published online October 31, 2024
DOI: https://doi.org/10.4150/jpm.2024.00248
  • 334 View
  • 6 Download
AbstractAbstract PDF
The mechanical performance of SiC/SiC composites is significantly influenced by the architecture of fiber reinforcement. Among the various fabrication methods, the nano-powder infiltration transition/eutectic (NITE) process is a promising technique that is capable of achieving a dense and stoichiometric SiC matrix. The reinforcement architecture, such as cross-ply (CP) or woven prepreg (WP), is determined during the preform stage of the NITE process, which is crucial in determining the mechanical properties of SiC/SiC composites. In this study, the tensile test and double notch shear (DNS) test were conducted using NITE-SiC/SiC composites to investigate the effect of the fiber reinforcing architecture on the fracture mechanism of SiC/SiC composites. The tensile strength and maximum shear strength of both CP and WP specimens were nearly identical. However, other mechanical properties, particularly those of CP specimens, exhibited significant variability. A comparison of fracture surfaces and load-displacement curve analyses from the DNS tests revealed that the cross points of the longitudinal or transverse fibers act as obstacles to both deformation and crack propagation. These obstacles were found to be more densely distributed in WP specimens than in CP specimens. The variability observed in the mechanical properties of CP specimens is likely due to size effects caused by the sparser distribution of these obstacles compared to the WP specimens.
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[English]
Machine Learning Modeling of the Mechanical Properties of Al2024-B4C Composites
Maurya A. K., Narayana P. L., Wang X.-S., Reddy N. S.
J Powder Mater. 2024;31(5):382-389.   Published online October 31, 2024
DOI: https://doi.org/10.4150/jpm.2024.00234
  • 463 View
  • 16 Download
AbstractAbstract PDF
Aluminum-based composites are in high demand in industrial fields due to their light weight, high electrical conductivity, and corrosion resistance. Due to its unique advantages for composite fabrication, powder metallurgy is a crucial player in meeting this demand. However, the size and weight fraction of the reinforcement significantly influence the components' quality and performance. Understanding the correlation of these variables is crucial for building high-quality components. This study, therefore, investigated the correlations among various parameters—namely, milling time, reinforcement ratio, and size—that affect the composite’s physical and mechanical properties. An artificial neural network model was developed and showed the ability to correlate the processing parameters with the density, hardness, and tensile strength of Al2024-B4C composites. The predicted index of relative importance suggests that the milling time has the most substantial effect on fabricated components. This practical insight can be directly applied in the fabrication of high-quality Al2024-B4C composites.
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[Korean]
Fabrication of 3D Aligned h-BN based Polymer Composites with Enhanced Mechanical Properties for Battery Housing
Kiho Song, Hyunseung Song, Sang In Lee, Changui Ahn
J Powder Mater. 2024;31(4):329-335.   Published online August 30, 2024
DOI: https://doi.org/10.4150/jpm.2024.00220
  • 683 View
  • 24 Download
AbstractAbstract PDFSupplementary Material
As the demand for electric vehicles increases, the stability of batteries has become one of the most significant issues. The battery housing, which protects the battery from external stimuli such as vibration, shock, and heat, is the crucial element in resolving safety problems. Conventional metal battery housings are being converted into polymer composites due to their lightweight and improved corrosion resistance to moisture. The transition to polymer composites requires high mechanical strength, electrical insulation, and thermal stability. In this paper, we proposes a high-strength nanocomposite made by infiltrating epoxy into a 3D aligned h-BN structure. The developed 3D aligned h-BN/epoxy composite not only exhibits a high compressive strength (108 MPa) but also demonstrates excellent electrical insulation and thermal stability, with a stable electrical resistivity at 200 °C and a low thermal expansion coefficient (11.46ⅹppm/℃), respectively.
Review Paper
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[English]
Research Trends in Electromagnetic Shielding using MXene-based Composite Materials
Siyeon Kim, Jongmin Byun
J Powder Mater. 2024;31(1):57-76.   Published online February 28, 2024
DOI: https://doi.org/10.4150/KPMI.2024.31.1.57
  • 2,734 View
  • 110 Download
  • 2 Citations
AbstractAbstract PDF

Recent advancements in electronic devices and wireless communication technologies, particularly the rise of 5G, have raised concerns about the escalating electromagnetic pollution and its potential adverse impacts on human health and electronics. As a result, the demand for effective electromagnetic interference (EMI) shielding materials has grown significantly. Traditional materials face limitations in providing optimal solutions owing to inadequacy and low performance due to small thickness. MXene-based composite materials have emerged as promising candidates in this context owing to their exceptional electrical properties, high conductivity, and superior EMI shielding efficiency across a broad frequency range. This review examines the recent developments and advantages of MXene-based composite materials in EMI shielding applications, emphasizing their potential to address the challenges posed by electromagnetic pollution and to foster advancements in modern electronics systems and vital technologies.

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  • Designing dual phase hexaferrite (SrFe12O19) – Perovskite (La0.5Nd0.5FeO3) composites for enhanced electromagnetic wave absorption and band gap modulation
    Pramod D. Mhase, Varsha C. Pujari, Santosh S. Jadhav, Abdullah G. Al-Sehemi, Sarah Alsobaie, Sunil M. Patange
    Composites Communications.2025; 54: 102284.     CrossRef
  • Microstructure tailoring of Nb-based MAX phase by low temperature synthesis with layer-structured Nb2C powder and molten salt method
    Chaehyun Lim, Wonjune Choi, Jongmin Byun
    Materials Characterization.2025; 225: 115106.     CrossRef
Articles
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[Korean]
Phase Formation and Mechanical Property of YSZ‒30 vol.% WC Composite Ceramics Fabricated by Hot Pressing
Jin-Kwon Kim, Jae-Hyeong Choi, Nahm Sahn, Sung-Soo Ryu, Seongwon Kim
J Powder Mater. 2023;30(5):409-414.   Published online October 1, 2023
DOI: https://doi.org/10.4150/KPMI.2023.30.5.409
  • 275 View
  • 3 Download
AbstractAbstract PDF

YSZ (Y2O3-stabilized zirconia)-based ceramics have excellent mechanical properties, such as high strength and wear resistance. In the application, YSZ is utilized in the bead mill, a fine-grinding process. YSZ-based parts, such as the rotor and pin, can be easily damaged by continuous application with high rpm in the bead mill process. In that case, adding WC particles improves the tribological and mechanical properties. YSZ-30 vol.% WC composite ceramics are manufactured via hot pressing under different pressures (10/30/60 MPa). The hot-pressed composite ceramics measure the physical properties, such as porosity and bulk density values. In addition, the phase formation of these composite ceramics is analyzed and discussed with those of physical properties. For the increased applied pressure of hot pressing, the tetragonality of YSZ and the crystallinity of WC are enhanced. The mechanical properties indicate an improved tendency with the increase in the applied pressure of hot pressing.

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[Korean]
Fabrication of Polymer Composite with Enhanced Insulation and Mechanical Properties using Aluminum Borate Nanowhiskers
Junhyeok Choi, Sangin Lee, Kiho Song, Taekyung Kim, Changui Ahn
J Powder Mater. 2023;30(4):356-362.   Published online August 1, 2023
DOI: https://doi.org/10.4150/KPMI.2023.30.4.356
  • 476 View
  • 2 Download
  • 1 Citations
AbstractAbstract PDF

Inorganic-organic composites find extensive application in various fields, including electronic devices and light-emitting diodes. Notably, encapsulation technologies are employed to shield electronic devices (such as printed circuit boards and batteries) from stress and moisture exposure while maintaining electrical insulation. Polymer composites can be used as encapsulation materials because of their controllable mechanical and electrical properties. In this study, we propose a polymer composite that provides good electrical insulation and enhanced mechanical properties. This is achieved by using aluminum borate nanowhiskers (ABOw), which are fabricated using a facile synthesis method. The ABOw fillers are created via a hydrothermal method using aluminum chloride and boric acid. We confirm that the synthesis occurs in various morphologies based on the molar ratio. Specifically, nanowhiskers are synthesized at a molar ratio of 1:3 and used as fillers in the composite. The fabricated ABOw/epoxy composites exhibit a 48.5% enhancement in mechanical properties, similar to those of pure epoxy, while maintaining good electrical insulation.

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  • Fabrication of Al18B4O33 Spherical Powder with Increased Fluidity via Control of B2O3 Particle Size and Distribution
    Kiho Song, Sang in Lee, Hyunseung Song, Changui Ahn
    Journal of Powder Materials.2024; 31(6): 513.     CrossRef
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[Korean]
Epoxy-Based Siloxane/Silica Composites for Electronic Packaging by Composition and Molecular Structure of Siloxane, and Analysis of Changes in Properties
Junho Jang, Dong Jun Kang, Hyeon-Gyun Im
J Powder Mater. 2023;30(4):346-355.   Published online August 1, 2023
DOI: https://doi.org/10.4150/KPMI.2023.30.4.346
  • 439 View
  • 7 Download
  • 1 Citations
AbstractAbstract PDF

Epoxy-based composites find extensive application in electronic packaging due to their excellent processability and insulation properties. However, conventional epoxy-based polymers exhibit limitations in terms of thermal properties and insulation performance. In this study, we develop epoxy-based siloxane/silica composites that enhance the thermal, mechanical, and insulating properties of epoxy resins. This is achieved by employing a sol–gelsynthesized siloxane hybrid and spherical fused silica particles. Herein, we fabricate two types of epoxy-based siloxane/ silica composites with different siloxane molecular structures (branched and linear siloxane networks) and investigate the changes in their properties for different compositions (with or without silica particles) and siloxane structures. The presence of a branched siloxane structure results in hardness and low insulating properties, while a linear siloxane structure yields softness and highly insulating properties. Both types of epoxy-based siloxane/silica composites exhibit high thermal stability and low thermal expansion. These properties are considerably improved by incorporating silica particles. We expect that our developed epoxy-based composites to hold significant potential as advanced electronic packaging materials, offering high-performance and robustness.

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  • Enhanced Epoxy Composites Reinforced by 3D-Aligned Aluminum Borate Nanowhiskers
    Hyunseung Song, Kiho Song, Haejin Hwang, Changui Ahn
    Materials.2024; 17(19): 4727.     CrossRef
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[Korean]
Experimental Study on Improving Thermal Shock Resistance of Cement Composite Incorporating Hollow Glass Microspheres
Yomin Choi, Hyun‐Gyoo Shin
J Powder Mater. 2022;29(6):505-510.   Published online December 1, 2022
DOI: https://doi.org/10.4150/KPMI.2022.29.6.505
  • 264 View
  • 2 Download
AbstractAbstract PDF

The thermal shock resistance of cement composites with hollow glass microspheres (HGM) is investigated. Cement composites containing various concentrations of HGM are prepared and their properties studied. The density, thermal conductivity, and coefficient of thermal expansion of the composites decrease with increasing HGM concentration. A thermal shock test is performed by cycling between -60 and 50ºC. After the thermal shock test, the compressive strength of the cement composite without HGM decreases by 28.4%, whereas the compressive strength of the cement composite with 30 wt% HGM decreases by 5.7%. This confirms that the thermal shock resistance of cement is improved by the incorporation of HGM. This effect is attributed to the reduction of the thermal conductivity and coefficient of thermal expansion of the cement composite because of the incorporation of HGM, thereby reducing the occurrence of defects due to external temperature changes.

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[Korean]
Comparison of Properties with Different Sintering Process of 3Y-TZP/WC Composites
Min-Soo Nam, Jae-Hyung Choi, Sahn Nahm, Seongwon Kim
J Powder Mater. 2022;29(5):424-431.   Published online October 1, 2022
DOI: https://doi.org/10.4150/KPMI.2022.29.5.424
  • 419 View
  • 2 Download
  • 1 Citations
AbstractAbstract PDF

3Y-TZP ceramics obtained by doping 3 mol.% of Y2O3 to ZrO2 to stabilize the phase transition are widely used in the engineering ceramic industry due to their excellent mechanical properties such as high strength, fracture toughness, and wear resistance. An additional increase in mechanical properties is possible by manufacturing a composite in which a high-hardness material such as oxide or carbide is added to the 3Y-TZP matrix. In this study, composite powder was prepared by dispersing a designated percentage of WC in the 3Y-TZP matrix, and the results were compared after manufacturing the composite using the different processes of spark plasma sintering and HP. The difference between the densification behavior and porosity with the process mechanism was investigated. The correlation between the process conditions and phase formation was examined based on the crystalline phase formation behavior. Changes to the microstructure according to the process conditions were compared using field-emission scanning electron microscopy. The toughness-strengthening mechanism of the composite with densification and phase formation was also investigated.

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  • Phase Formation and Mechanical Property of YSZ‒30 vol.% WC Composite Ceramics Fabricated by Hot Pressing
    Jin-Kwon Kim, Jae-Hyeong Choi, Nahm Sahn, Sung-Soo Ryu, Seongwon Kim
    journal of Korean Powder Metallurgy Institute.2023; 30(5): 409.     CrossRef
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[Korean]
Interfacial Reaction between Spark Plasma Sintered High-entropy Alloys and Cast Aluminum
Min-Sang Kim, Hansol Son, Cha Hee Jung, Juyeon Han, Jung Joon Kim, Young-Do Kim, Hyunjoo Choi, Se Hoon Kim
J Powder Mater. 2022;29(3):213-218.   Published online June 1, 2022
DOI: https://doi.org/10.4150/KPMI.2022.29.3.213
  • 337 View
  • 3 Download
  • 1 Citations
AbstractAbstract PDF

This study investigates the interfacial reaction between powder-metallurgy high-entropy alloys (HEAs) and cast aluminum. HEA pellets are produced by the spark plasma sintering of Al0.5CoCrCu0.5FeNi HEA powder. These sintered pellets are then placed in molten Al, and the phases formed at the interface between the HEA pellets and cast Al are analyzed. First, Kirkendall voids are observed due to the difference in the diffusion rates between the liquid Al and solid HEA phases. In addition, although Co, Fe, and Ni atoms, which have low mixing enthalpies with Al, diffuse toward Al, Cu atoms, which have a high mixing enthalpy with Al, tend to form Al–Cu intermetallic compounds. These results provide guidelines for designing Al matrix composites containing high-entropy phases.

Citations

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  • Simultaneous enhancement of strength and ductility of Al matrix composites enabled by submicron-sized high-entropy alloy phases
    Chahee Jung, Seungin Nam, Hansol Son, Juyeon Han, Jaewon Jeong, Hyokyung Sung, Hyoung Seop Kim, Seok Su Sohn, Hyunjoo Choi
    Journal of Materials Research and Technology.2024; 33: 1470.     CrossRef
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[Korean]
Preparation of CoFe2O4 Nanoparticle Decorated on Electrospun Carbon Nanofiber Composite Electrodes for Supercapacitors
Hyewon Hwang, Seoyeon Yuk, Minsik Jung, Dongju Lee
J Korean Powder Metall Inst. 2021;28(6):470-477.   Published online December 1, 2021
DOI: https://doi.org/10.4150/KPMI.2021.28.6.470
  • 288 View
  • 4 Download
AbstractAbstract PDF

Energy storage systems should address issues such as power fluctuations and rapid charge-discharge; to meet this requirement, CoFe2O4 (CFO) spinel nanoparticles with a suitable electrical conductivity and various redox states are synthesized and used as electrode materials for supercapacitors. In particular, CFO electrodes combined with carbon nanofibers (CNFs) can provide long-term cycling stability by fabricating binder-free three-dimensional electrodes. In this study, CFO-decorated CNFs are prepared by electrospinning and a low-cost hydrothermal method. The effects of heat treatment, such as the activation of CNFs (ACNFs) and calcination of CFO-decorated CNFs (C-CFO/ACNFs), are investigated. The C-CFO/ACNF electrode exhibits a high specific capacitance of 142.9 F/g at a scan rate of 5 mV/s and superior rate capability of 77.6% capacitance retention at a high scan rate of 500 mV/s. This electrode also achieves the lowest charge transfer resistance of 0.0063 Ω and excellent cycling stability (93.5% retention after 5,000 cycles) because of the improved ion conductivity by pathway formation and structural stability. The results of our work are expected to open a new route for manufacturing hybrid capacitor electrodes containing the C-CFO/ACNF electrode that can be easily prepared with a low-cost and simple process with enhanced electrochemical performance.

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[Korean]
Microstructures and Mechanical Properties of Ti-20Mo-0.5EB Composites
Suhyun Bae, Wonki Jeong, Se-Eun Shin
J Korean Powder Metall Inst. 2021;28(5):403-409.   Published online October 1, 2021
DOI: https://doi.org/10.4150/KPMI.2021.28.5.403
  • 275 View
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AbstractAbstract PDF

In this study, Ti-Mo-EB composites are prepared by ball milling and spark plasma sintering (SPS) to obtain a low elastic modulus and high strength and to evaluate the microstructure and mechanical properties as a function of the process conditions. As the milling time and sintering temperature increased, Mo, as a β-Ti stabilizing element, diffused, and the microstructure of β-Ti increased. In addition, the size of the observed phase was small, so the modulus and hardness of α-Ti and β-Ti were measured using nanoindentation equipment. In both phases, as the milling time and sintering temperature increased, the modulus of elasticity decreased, and the hardness increased. After 12 h of milling, the specimen sintered at 1000°C showed the lowest values of modulus of elasticity of 117.52 and 101.46 GPa for α-Ti and β-Ti, respectively, confirming that the values are lower compared to the that in previously reported studies.


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